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Sample Preparation: Power-Prep™ System

DescriptionApplicationsMethodsSpecificationsPhotograph

DESCRIPTION

 

Power-Prep™ System


The Power-Prep™ is a high speed sample processing workstation. It is designed to automate the extraction and cleanup of toxic compounds such as Dioxins, PCBs, Pesticides, and PAHs from environmental, biological and food samples.

Power-Prep processes from 1 to 10 samples in less than 1 hour, thereby, achieving high recoveries and excellent precision for all target compounds.

The Power-Prep™ system fits into the smallest budget. With its modular design, you can cost effectively automate your extraction and sample clean-up procedures by purchasing a 1-sample system and expand it to 5 or 10 samples as needed.

 

PRINCIPLES OF OPERATION

 

Power-Prep™ is changing the face of high speed sample processing in today's laboratories. The computer controlled liquid chromatography system performs simultaneous sample processing  automatically and unattended. You need only to load your samples, snap on your pre-packed columns and press the start key. The system performs the entire extraction and cleanup automatically including sample loading, washing, elution and fraction collection.

The Power-Prep™ system separates Dioxins, PCBs, and Pesticides for 5 samples in less than one hour.

Software

 

FMS’s powerful windows-based monitoring and control software offers a rich set of features and flexibility. It includes functions to develop and optimize methods.

Input parameter include flow rates, volumes, column selection, sample size, solvent selection and fraction collection

 

Hardware


Each Power-Prep™ system contains multiple quick connect modules consisting of:

  • Power Supply Module
  • Control Module
  • Pump & Pressure Modules
  • Valve Drive Modules
  • Sample Processing Modules

 

The Power-Prep modules are mounted vertically on a portable cabinet. It is a self contained system that also provides storage for solvent bottles, waste and collectors.


Modular and Expandable

 

A one-sample PowerPrep system can be expanded up to a 10 sample configuration. Both expansion and module replacement are done via FMS’s quick connect modules. This feature reduces system down time and increases laboratory throughput.



Applications

Sample Clean-Up

The Power-Prep sample clean-up system separates Dioxins, PCBs, and Pesticides from a variety of sample extracts such as:

    • Soils
    • Water
    • Fly Ash
    • Milk
    • Air
    • Waste
    • Human Serum
    • Adipose Tissue
    • Fish Samples
    • Waste Water
    • Pulp & Paper

 

Solid Phase Extraction (SPE)

In addition to sample clean-up the Power-Prep automates the entire Solid Phase Extraction of Dioxins, PCBs and Pesticides from a variety of aqueous samples such as:

    • Water
    • Milk
    • Waste Water
    • Human Serum

 

Saves Time & Money


With a few keystrokes, the Power-Prep system performs an entire column chromatography, automatically achieving high recoveries for all analytes. The unattended operation feature of the system saves labor and valuable time.
The Power-Prep system reduces the amount of glassware and solvents required for manual sample clean-up.

Uses Disposable Columns


The Power-Prep System uses pre packed disposable columns. FMS’s proprietary columns are made from teflon and contain multi layer silica, alumina, and carbon. FMS’s prepacked columns are tested for purity and performance prior to shipment.


Yields High Recoveries


The combination of FMS’s patented pump controller and patented prepacked disposable teflon columns produces high recoveries for all analytes.


The following are typical recoveries using a spiked sample:

 

2378 - TCDD

75

2378 - TCDF

70

12378 - PeCDD

80

12378 - PeCDF

80

23478 - PeCDF

84

123478 - HXCDD

91

123678 - HXCDD

78

123789 - HXCDD

87

123478 - HXCDF

86

123678 - HXCDF

85

123789 - HXCDF

90

234678 - HXCDF

82

1234678 - HpCDF

82

1234678 - HXCDF

89

OCDD

74

OCDF

74

3344 - PCB (PCB 77)

78

3445 - PCB (PCB81)

82

33445 - PCB (PCB 126)

85

334455 - PCB (PCB169)

77

 

System Configuration

 

Power-Prep™/p (Parallel)
Parallel sample clean-up System for Dioxins, PCBs and Pesticides sample analysis.
Capacity:            1 to 10 samples
Processing time:  1 hour per run
Columns:

o        Multi-layer Silica

o        Alumina

o        Carbon

Column Material: Teflon

Power-Prep™/s (Sequential)
Sequential sample clean-up System for Dioxins, PCBs and Pesticides sample analysis.
Capacity:             5 samples
Processing time:   5 hours per run
Columns:

o        Multi-layer Silica

o        Alumina

o        Carbon

Column Material: Teflon

Power-Prep™/SPE
Automated Solid Phase Extraction System for automating EPA, SW-846 methods for pesticides, PCBs and PAHs sample analysis

 Capacity:            5 to 25 samples
Processing time:  1 to 5 hours per run
Columns:

o        Silica

o        Alumina

o        Carbon

o        Florisil

o        C18

Column Material: Teflon, Polypropylene

Power-Prep™/GPC
Automated GPC Clean-up System for automating EPA, SW-846 GPC Clean-up method for pesticides, PCBs and PAHs sample analysis.
Capacity: 5 to 25 samples
Processing time: 5 to 25 hours per run
Packing Material: Styrene-DiVinylBenzene
Column Material: Teflon, Glass

 

For additional Information please Visit Power-Prep web site

 

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