Automated Sample Preparation
ASE Pressurized Liquid Extraction (PLE)
An overview
Overview of ASE Pressurized Liquid Extraction (PLE)
What is Pressurized Liquid Extraction?
Pressurized Liquid Extraction (PLE), also known as Accelerated Solvent Extraction (ASE) , is an advanced sample extraction technique. It utilizes liquid solvents under elevated temperatures and pressures to prepare samples for analysis using gas chromatography (GC) or liquid chromatography (LC). Unlike traditional Soxhlet extraction, PLE allows the solvent within the extraction cell to approach the supercritical region, resulting in more efficient extractions.
The elevated temperature enhances solubility and increases the diffusion rate of the sample. Simultaneously, the high pressure ensures the solvent remains below its boiling point, allowing it to penetrate solid samples more effectively. This approach significantly reduces solvent usage.
Benefits of Pressurized Liquid Extraction
When compared to Soxhlet extraction, PLE demonstrates remarkable efficiency. Extraction time is reduced from 18 hours to just 22 minutes. Furthermore, solvent consumption decreases from 300 mL to 80 mL or less of organic solvent.
How Does Pressurized Liquid Extraction Work?
To perform PLE, a sample weighing between 5 grams and 100 grams is mixed with sodium sulfate. The mixture is then placed in an extraction cell capped with filtration end fittings. Once loaded into the PLE™ system, the process automatically begins:
- The system heats and pressurizes the sample.
- Pressure is maintained between 1500-3000 PSI, with temperatures ranging from 70-200°C.
- The extracted solvent, containing target analytes, is transferred to a concentration/evaporation vessel.
The final concentrated sample is collected in a GC or LC vial, ready for analys
PLE Applications
Automated Sample Preparation for Dioxins and Furans in Stack Emissions
Total Extractable Fat using Pressurized Liquid Extraction (PLE)
EPA 1613 PCDD-Fs in Cranberry Pulp by PLE and PowerPrep
EPA 1613 PCDD-Fs and PCBs Analysis in Pet Food Using Automated Extraction and Cleanup
EPA 8081B Toxaphene in Fish by PLE and PowerPrep
EPA 1613 Dioxins and Furans in Freeze-Dried and Regular Milk by PLE and PowerPrep
EPA 1613 Dioxins and Furans in Egg Yolk by PLE
EPA 1613 Dioxins and Furans in Crab Meat by PowerPrep and PLE
EPA 1613 and 1668C POPs Extraction and CleanUp using Low Solvent Green Total EconoPrep
EPA 1613 and 1668 PCDDs PCDFs and PCBs in Fish by Automated Sample Processing
EPA 1613 and 1668 Dioxins PCBs and PBDEs in Human Serum by PLE and PowerPrep
EPA 1613 and 1668 Dioxins Furans and PCBs in Peanut Butter Samples by PLE and PowerPrep
EPA 1668 PCBs in Coffee via PLE and Reduced Volume Cleanup
A Quick Screen Method for the Extraction, Cleanup and Concentration of Toxaphene in Fish
One Step Extraction, Cleanup and Direct-to-Vial Concentration For PCBs in Soil and Sediment
One Step Extraction, Cleanup and Concentration of Pesticides from Soil
One Step Extraction, Cleanup and Concentration of Chlorinated Pesticides in Raw Coffee Beans
Pressurized Liquid Extraction of Soil Samples for the Analysis of Diesel Range Organics by GC/FID
Total Extractable Fat Using Pressurized Liquid Extraction (PLE)
Polychlorinated Dibenzo-p-dioxins, Furans and Biphenyls in Fish Automated Sample Processing
The Analysis of Chlorinated Dioxins, Difurans in Pet Food
Automated Extraction and Cleanup of Egg Yolk Dioxins and Furans
Automated Extraction and Clean Up of Crab Meat Dioxins and Furans
Dioxins, Furans, and PCBs in Peanut Butter Samples Processed with Automated Extraction and Clean Up
One Step Extraction, Cleanup and Concentration for PBDEs in Soil
Automated Extraction and Clean Up of Wood Boiler Ash Samples Dioxins, Furans, and PCBs
PLE US EPA Approval Letter
Product Video
Details
Pressurized Liquid Extraction (PLE) System
The PLE® system is a high-speed pressurized liquid extraction system designed to perform sample extraction of multiple samples simultaneously. The PLE system delivers high recoveries and excellent precision for all analytes in minutes instead of hours. Inexpensive stainless steel extraction cells with end cap filtration keep operational costs at a minimum. Optional disposable end cap filtration increases productivity and saves valuable time.
Reduce Solvent Costs
Pressurized liquid extraction uses as little as 15 mL of solvent compared to more than 500 mL of solvent required to perform Soxhlet extractions.
Reduce Solvent Waste
The PLE system reduces solvent waste by using solvents more efficiently.
Increase Productivity
The entire extraction and cleanup may be performed in less than 30 minutes. Traditional methods can take 10 to 16 hours.
Reduce Operating Costs
Rapid extraction and clean-up, along with reduced solvent use and waste, reduces operating costs by as much as 70 percent.
Five to 250 mL Extraction Cell Sizes
The PLE™ system offers 5-250 mL low cost stainless steel extraction cells with Teflon endcap filtration. This wide range of extraction cell volumes allows the use of the same unit for all sample sizes, even in the same run.
Modular, Expandable and Affordable
The modular design of the PLE system allows you to purchase a one, two or three sample system to fit your budget. The system can be expanded to a five or six sample system as your application grows.
Eliminate cross contamination
Optional low-cost disposable extraction cells and Teflon filtration endcaps ensure trouble-free extraction and eliminate the risk of cross contamination.
One-Step Sample Extraction and Cleanup
The optional in-line cleanup module performs the entire sample extraction and cleanup in one step with increased speed and reduced cost.
Automatic Operation and Documentation
Real-time software allows six channels of pressure and six channels of temperature data to be plotted simultaneously. This powerful feature allows automatic documentation of all extraction data. Temperature and pressure data can be superimposed and printed in either graphic or tabular format and stored for future reference.
Modular Construction Provides for Easy Maintenance
The modular desgin of the PLE sytem combined with its exposed plumbing enables efficient system maintenance. The PLE system’s channels are designed to operate independently, so if one channel fails the others will continue to perform. This versatility ensures easy replacement with no down time.
Leak and Clog Free Operation
Simple design combined with large bore plumbing enables the PLE system to operate virtually leak and clog free.
Multiple Extractions
Programming of variable pressure and temperature allows extraction of a variety of compounds.
Specifications
Technical Specification
| Extraction cell size: | 5 mL, 10 mL, 20 mL, 40 mL, 70 mL, 100 mL, 250 mL |
| Simultaneous Extractions | 1 to 6 independent extraction modules for simultaneous extraction |
| Variable Cell Size per Simultaneous Extraction Run | Run different cell sizes in the same simultaneous run 5 mL, 10 mL, 20 mL, 40 mL, 70 mL, 100 mL or 250 mL |
| Modular Design | Individual Extraction Modules can be isolated from the system without interrupting the running system, no down time. |
| Automated Sample Cleanup | Incell Sample Cleanup, Pre-packed Incell End Cap Sample Cleanup, Inline Column Sample Cleanup, |
| Interface to Automated Cleanup Systems | Seamless programmable interface to PowerPrep™ Multi-Column Sample Cleanup System |
| Interface to Automated Concentration Systems | Seamless Programmable interface to the SuperVap Concentrator to provide one step extraction and concentration or one step extraction, sample cleanup and concentration |
| Flow Rate | 0 to 35 mL per minute |
| Pressure | 0 to 2500 PSI |
| Temperature | Ambient to 200 ºC |
| Solvents | No limitation, mixing or selection of up to six different solvents |
| Collection Vessels | Direct to a SuperVap Concentration Vessel or SuperVap Direct to GC Vial Concentration Vessel. All other standard collection vessels. |
| Automatic Documentation | The DMS-6000 software allows multiple methods to be stored. Each parameter such as time, solvent volume, and final temperature can be set for each step. Pressure, temperature and dispensed volumes are displayed real time. All parameters for each run are documented and stored for future reference. |
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DMS 6000 Software
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The PLE™ system uses a PC to control the entire extraction, sample cleanup and concentration process. The DMS-6000 real time software allows multiple samples to be processed simultaneously. |
| Recoveries and Reproducibility | Method compliance or better |
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Real Time Monitoring, Plotting of Pressure and Temperature
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The DMS-6000 real time software allows six channels of pressure and six channels of temperature to be plotted in real time. This powerful feature allows automatic documentation of the entire extraction data. The temperature and pressure can be superimposed and printed in graphic or tabular format. |
| One Step Automated Extraction, Sample Clean up and Concentration Control Software | Used to write, and edit extraction protocols, monitor, and store the extraction, ample cleanup and concentration data. It also controls the entire sample prep process. |
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Automatic Extraction Data Report
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The DMS-6000 real time software allows the creation of an automatic data report based on the sample sequence set up. Printed data contains the graph and parameters of the sample extraction. |
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Weights: PLE Pump module = 10 lbs PLE Control module = 15 lbs PLE valve module = 15 lbs PLE structure = 27 lbs PLE Large cabinet = 18 lbs PLE small cabinet = 24 lbs PC = 21 lbs Monitor = 10 lbs |
Weights: Small cart = 35 lbs Small tray = 20 lbs Medium cart = 40 lbs Medium tray = 25 lbs Large cart = 45 lbs Large tray = 35 lbs
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Small cabinet + pump module + control module = 50 lbs Large cabinet + valve module + structure = 60 lbs PC + monitor = 30 lbs PLE1 = 110 lbs + 30 lbs = 140 lbs PLE2 = 170 lbs + 30 lbs = 200 lbs PLE3 = 230 lbs + 30 lbs = 260 lbs PLE4 = 290 lbs + 30 lbs = 320 lbs PLE5 = 350 lbs + 30 lbs = 380 lbs PLE6 = 410 lbs + 30 lbs = 440 lbs |
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Dimensions: PLE1 = 15” (38 cm) W X 35” (90 cm) H X 18” (45 cm) D PLE2 = 23” (58 cm) W X 35” (90 cm) H X 18” (45 cm) D PLE3 = 31” (78 cm) W X 35” (90 cm) H X 18” (45 cm) D PLE4 = 39” (98 cm) W X 35” (90 cm) H X 18”(45 cm) D PLE5 = 47” (118 cm) W X 35” (90 cm) H X 18” (45 cm) D PLE6 = 55” (138 cm) W X 35” (90 cm) H X 18” (45 cm) D
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Dimensions with cart and tray: PLE2 = 37” (94 cm) W X 64” (162 cm) H X 30” (75 cm) D PLE3 = 45” (114 cm) W X 64” (162 cm) H X 30” (75 cm) D PLE4 = 64” (162 cm) W X 64” (162 cm) H X 30” (75 cm) D PLE5 = 64” (162 cm) W X 64” (162 cm) H X 30” (75 cm) D PLE6 = 64” (162 cm) W X 64” (162 cm) H X 30” (75 cm) D
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Consumables
| Extraction Cartridges | |
| PLE-CAR-SS10 | 10ml stainless steel PLE cartridge |
| PLE-CAR-SS20 | 20ml stainless steel PLE cartridge |
| PLE-CAR-SS40 | 40ml stainless steel PLE cartridge |
| PLE-CAR-SS100 | 100ml stainless steel PLE cartridge |
| PLE-WSH-CLL | PLE wash column, large |
| PLE-WSH-CLS | PLE wash column, small |
| Cartridge End Caps | |
| PLE-FLT-100M-TEF-NP | Teflon cap filtration for PLE cartridge-non polar solvents |
| PLE-FLT-100M-TEF-P | Teflon cap filtration for PLE cartridge-polar solvents |
| PLE-FLT-100M-TEF-U | Teflon cap filtration for PLE cartridge-Universal |
| PLE-FLT-100M-TEF-NO | Teflon cap filtration for PLE cartridge-no O-ring |
| PLE-FLT-100M-SS-NP | Reusable Stainless Steel End cap filtration for PLE cartridge- non polar solvents |
| PLE-FLT-100M-SS-P | Reusable Stainless Steel End cap filtration for PLE cartridge-polar solvents |
| PLE-FLT-100M-SS-U | Reusable Stainless Steel End cap filtration for PLE cartridge-Universal |
| PLE-FLT-100M-SS | Reusable Stainless Steel End cap filtration for PLE cartridge-not assembled |
| O-rings & Filters | |
| PLE-OR-ETP-ST | Viton ETP (universal) Orings Set: size 014, 017, 116 |
| PLE-OR-NEO-ST | Neoprene (Polar) Orings Set: size 014, 017, 116 |
| PLE-OR-VIT-ST | Viton (non polar) Orings Set: size 014, 017, 116 |
| PLE-SS-FLT-10 | Stainless Steel Filter |
| PLE-SS-RET | Retaining ring |
| Tools | |
| PLE-RET-TL | Retaining ring tool |
| PLE-TL-SET | PLE Tool set |
PLE for food testing
Integrated Sample Extraction and Cleanup Ready for the Analysis of Potency and Pesticides in Cannabis
Extraction of Pesticides in Cannabis: High-Speed Pesticide Analysis in Cannabis using ASE PLE
The PLE Cannabis Extraction System is an advanced pressurized liquid extraction system designed for the efficient extraction of multiple compounds, including cannabinoids, from cannabis oil. This system offers exceptional speed, delivering high recoveries and yields with outstanding precision in minutes—significantly faster than traditional extraction methods that take hours.
Key Features of the PLE Cannabis Extraction System
- Efficiency and Precision: The PLE system ensures precise extraction of all cannabinoids, achieving high recoveries with minimal solvent usage.
- Cost-Effective Operation: Durable, stainless steel extraction cells with reusable end cap filtration minimize operational costs and reduce waste.
- Enhanced Productivity: The reusable end cap filtration system increases throughput by eliminating downtime, making it ideal for high-volume operations.
- Streamlined Cleanup: The PLE system incorporates a unique supercooling feature that simplifies the cleanup process. This eliminates extra manual steps required by other techniques, reducing human interaction while boosting overall efficiency.
How It Works:
The PLE system uses pressurized liquid extraction technology, leveraging elevated temperatures and pressures for efficient extraction. Solvents under controlled conditions penetrate the cannabis material more effectively, ensuring optimal cannabinoid recovery.
- Pressure Range: Operates at 1500-3000 PSI.
- Temperature Control: Adjustable from 70°C to 200°C for tailored extraction conditions.
- Automation: Automatically extracts, concentrates, and transfers samples directly to vials, ready for analysis or further processing.
Why Choose PLE for Cannabis Extraction?
Compared to conventional methods, the PLE system drastically reduces extraction time while improving precision and consistency. Its innovative design ensures that every step, from extraction to cleanup, is optimized for maximum throughput, enabling businesses to scale operations without compromising on quality.
• One extraction method for all matrices
• High Speed
• Modular and expandable from 1 to 8
• Process 1 to 8 samples in 10 to 15 min
• Extraction cell size 5 to 200 ml
• Real time plot of temperature and pressure
• Reduced Solvent Consumption
• Works efficiently on all Sample Matrices
• Lower Energy Consumption
• InCell Sample Cleanup
PLE – Cannabis Applications
Product Video
Details
Modular, Expandable and Affordable from 1 to 8 modules
The modular design of the PLE system allows you to purchase a one, two up to eight sample system to fit your budget. The system can be expanded from a one to eight sample system as your work load grows.
The modular design of the PLE system allows you to purchase a one, two up to eight sample system to fit your budget. The system can be expanded from a one to eight sample system as your work load grows.
Reduce Solvent Waste
The PLE system reduces solvent waste by using solvents more efficiently. Cut solvent consumption in half.
Increase Productivity
The entire extraction and cleanup is performed in minutes. Traditional methods can take hours.
Reduce Operating Costs
Rapid extraction and clean-up, along with reduced solvent use and waste, reduces operating costs by as much as 70 percent.
5 to 250 mL Extraction Cell Sizes
The PLE system offers 5-200 mL low cost stainless steel extraction cells with Teflon endcap filtration. This wide range of extraction cell volumes allows the use of the same unit for all sample sizes, even in the same run.
Eliminate cross contamination
Low-cost stainless steel extraction cells and Teflon filtration endcaps ensure trouble-free extraction and eliminate the risk of cross contamination.
Sample Extraction and Cleanup in one step
The PLE uses incell cleanup and performs the entire sample extraction and cleanup in one step with increased speed and reduced cost. Eliminating additional manual cleanup steps. Just inject the sample extract.
Automatic Operation and Documentation
Real-time software allows eight channels of pressure and eight channels of temperature data to be plotted simultaneously. Allows automatic documentation of all extraction data.
One Extraction Method for All Matrices
A single extraction method is used for Potency extractions for all sample types. A single extraction and cleanup method is used for all Pesticide extractions for all sample types. Eliminating the need to develop and validate several extraction protocols.
Specifications
| Extraction cell size: | 5 mL, 10 mL, 20 mL, 40 mL, 70 mL, 100 mL, 250 mL |
| Simultaneous Extractions | 1 to 6 independent extraction modules for simultaneous extraction |
| Variable Cell Size per Simultaneous Extraction Run | Run different cell sizes in the same simultaneous run 5 mL, 10 mL, 20 mL, 40 mL, 70 mL, 100 mL or 250 mL |
| Modular Design | Individual Extraction Modules can be isolated from the system without interrupting the running system, no down time. |
| Automated Sample Cleanup | Incell Sample Cleanup, Pre-packed Incell End Cap Sample Cleanup, Inline Column Sample Cleanup, |
| Interface to Automated Cleanup Systems | Seamless programmable interface to PowerPrep™ Multi-Column Sample Cleanup System |
| Interface to Automated Concentration Systems | Seamless Programmable interface to the SuperVap Concentrator to provide one step extraction and concentration or one step extraction, sample cleanup and concentration |
| Flow Rate | 0 to 35 mL per minute |
| Pressure | 0 to 2500 PSI |
| Temperature | Ambient to 200 ºC |
| Solvents | No limitation, mixing or selection of up to six different solvents |
| Collection Vessels | Direct to a SuperVap Concentration Vessel or SuperVap Direct to GC Vial Concentration Vessel. All other standard collection vessels. |
| Automatic Documentation | The DMS-6000 software allows multiple methods to be stored. Each parameter such as time, solvent volume, and final temperature can be set for each step. Pressure, temperature and dispensed volumes are displayed real time. All parameters for each run are documented and stored for future reference. |
| DMS 6000 Software | The PLE™ system uses a PC to control the entire extraction, sample cleanup and concentration process. The DMS-6000 real time software allows multiple samples to be processed simultaneously. |
| Recoveries and Reproducibility | Method compliance or better |
| Real Time Monitoring, Plotting of Pressure and Temperature | The DMS-6000 real time software allows six channels of pressure and six channels of temperature to be plotted in real time. This powerful feature allows automatic documentation of the entire extraction data. The temperature and pressure can be superimposed and printed in graphic or tabular format. |
| One Step Automated Extraction, Sample Clean up and Concentration Control Software | Used to write, and edit extraction protocols, monitor, and store the extraction, ample cleanup and concentration data. It also controls the entire sample prep process. |
| Automatic Extraction Data Report | The DMS-6000 real time software allows the creation of an automatic data report based on the sample sequence set up. Printed data contains the graph and parameters of the sample extraction. |
| Weights: | Weights: |
| PLE Pump module = 10 lbs | Small cart = 35 lbs |
| PLE Control module = 15 lbs | Small tray = 20 lbs |
| PLE valve module = 15 lbs | Medium cart = 40 lbs |
| PLE structure = 27 lbs | Medium tray = 25 lbs |
| PLE Large cabinet = 18 lbs | Large cart = 45 lbs |
| PLE small cabinet = 24 lbs | Large tray = 35 lbs |
| PC = 21 lbs | |
| Monitor = 10 lbs | |
| Small cabinet + pump module + control module = 50 lbs | |
| Large cabinet + valve module + structure = 60 lbs | |
| PC + monitor = 30 lbs | |
| PLE1 = 110 lbs + 30 lbs = 140 lbs | |
| PLE2 = 170 lbs + 30 lbs = 200 lbs | |
| PLE3 = 230 lbs + 30 lbs = 260 lbs | |
| PLE4 = 290 lbs + 30 lbs = 320 lbs | |
| PLE5 = 350 lbs + 30 lbs = 380 lbs | |
| PLE6 = 410 lbs + 30 lbs = 440 lbs | |
| Dimensions: | Dimensions with cart and tray: |
| PLE1 = 15” (38 cm) W X 35” (90 cm) H X 18” (45 cm) D | PLE2 = 37” (94 cm) W X 64” (162 cm) H X 30” (75 cm) D |
| PLE2 = 23” (58 cm) W X 35” (90 cm) H X 18” (45 cm) D | PLE3 = 45” (114 cm) W X 64” (162 cm) H X 30” (75 cm) D |
| PLE3 = 31” (78 cm) W X 35” (90 cm) H X 18” (45 cm) D | PLE4 = 64” (162 cm) W X 64” (162 cm) H X 30” (75 cm) D |
| PLE4 = 39” (98 cm) W X 35” (90 cm) H X 18”(45 cm) D | PLE5 = 64” (162 cm) W X 64” (162 cm) H X 30” (75 cm) D |
| PLE5 = 47” (118 cm) W X 35” (90 cm) H X 18” (45 cm) D | PLE6 = 64” (162 cm) W X 64” (162 cm) H X 30” (75 cm) D |
| PLE6 = 55” (138 cm) W X 35” (90 cm) H X 18” (45 cm) D |
Consumables
| Part # | Description |
| PLE-CAR-SS05 | 5ml stainless steel PLE cartridge |
| PLE-CAR-SS10 | 10ml stainless steel PLE cartridge |
| PLE-CAR-SS100 | 100ml stainless steel PLE cartridge |
| PLE-CAR-SS20 | 20ml stainless steel PLE cartridge |
| PLE-CAR-SS40 | 40ml stainless steel PLE cartridge |
| PLE-CAR-SS200 | 200ml Stainless Steel Cartridge |
PLE for Ethanol Extraction
Efficient, Fast, Safe Ethanol Extraction of Cannabis Oil
Integrated Ethanol Extraction, Cleanup and Oil Concentration Ready for Production
A single module PLE sending oil from 2 ounces of flower extracted directly to a SuperVap® Concentrator is capable of processing 4 lbs in 8 hrs. The PLE can be expanded up to 8 modules for extracting up to 8 modules in parallel, capable of processing 32 lbs. in 8 hrs.
• One Extraction Method for all Solvents
• High Speed, Extract in Minutes Not Hours
• Modular, Expandable and Scalable from 1 to 8 Extractors
• Process 2 oz. to 1 lb. in 10 min
• Extraction Cell Sizes 5 to 200 ml
• Real Time Plot of Temperature and Pressure
• Dramatically Reduces Solvent
• Works Efficiently
• Environmentally Safe Process
• Lower Energy Consumption
• Supercooled Solvent for Cleanup
• Optional Automated Evaporation
• Easy to Use Touch Screen
Details
The PLE system is a high-speed pressurized liquid extraction system designed to perform extraction of multiple compounds in the extraction of oil from cannabis simultaneously. The PLE system delivers high recoveries and yields with excellent precision of all cannabinoids in minutes instead of hours. Inexpensive stainless steel extraction cells with end cap filtration keep operational costs at a minimum. Reusable end cap filtration increases productivity and saves valuable time. Combining supercooling for cleanup eliminates extra manual cleanup steps required by other techniques increasing throughput while reducing human interaction.
HIGH SPEED EXTRACTIONS
- Most Efficient > 90%
- Highest Yield up to 30%
- 10 Minute Extraction
- Supercooled Cleanup
- From 4 Lbs. to 32 Lbs. in 8 Hrs.
Modular, Expandable and Affordable from 1 to 8 modules
The modular design of the PLE system allows you to purchase a one, two up to eight sample system to fit your budget. The system can be expanded from a one to eight sample system as your work load grows.
Reduce Solvent Waste
The PLE system reduces solvent waste by using solvents more efficiently. Cut solvent consumption in half.
Increase Productivity
The entire extraction and cleanup is performed in minutes. Traditional methods can take hours.
Reduce Operating Costs
Rapid extraction and clean-up, along with reduced solvent use and waste, reduces operating costs by as much as 70 percent.
5 to 200 mL Extraction Cell Sizes
The PLE system offers 5-200 mL low cost stainless steel extraction cells with Teflon endcap filtration. This wide range of extraction cell volumes allows the use of the same unit for all sample sizes, even in the same run.
Eliminate cross contamination
Low-cost stainless steel extraction cells and Teflon filtration endcaps ensure trouble-free extraction and eliminate the risk of cross contamination.
Sample Extraction and Cleanup in one step
The PLE uses incell cleanup and performs the entire sample extraction and cleanup in one step with increased speed and reduced cost. Eliminating additional manual cleanup steps. Just inject the sample extract.
Automatic Operation and Documentation
Real-time software allows eight channels of pressure and eight channels of temperature data to be plotted simultaneously. Allows automatic documentation of all extraction data.
One Extraction Method for All Matrices
A single extraction method is used for all cannabinoids and terpenes. A single extraction and cleanup method is used for extractions for all sample types. Eliminating the need to develop and validate several extraction protocols.
Specifications
| PLE/1 | PLE/2 | PLE/3 | PLE/4 |
| • Processes 1/2 lb. per hr. and 4 lbs. in 8 hrs. | • Processes 1 lb. per hr. and 8 lbs. in 8 hrs. | • Processes 1½ lbs. per hr. and 12 lbs. in 8 hrs | • Processes 2 lbs. per hr. and 16 lbs. in 8 hrs. |
| • Good for Home/Small Samples, Research and Product Development | • Good for Home/Small Samples, Research and Product Development | • Good for Small Operations or mobile | • Good for Small/Intermediate Operations or mobile applications |
| • Low Cost Entry level | • Low Cost Entry level | • Low Cost Business level | • Low Cost Business level |
| • Fully Automated | • Fully Automated | • Ideal for home operations/small samples, product development and R&D | • Fully Automated |
| • Smallest footprint (fits on a counter-top) | • Smallest footprint (fits on a counter-top) | • Fully Automated | • Smallest footprint (fits on a counter-top) |
| • Runs on 110V 20 amp circuit | • Runs on 110V 20 amp circuit | • Smallest footprint (fits on a counter-top) | • Runs on 110V 20 amp circuit |
| • Dimensions: 17” W X 26” H X 18” D | • Dimensions: 25” W X 26” H X 18” D | • Runs on 110V 20 amp circuit | • Dimensions: 41” W X 26” H X 18” D |
| • Dimensions: 33” W X 26” H X 18” D | |||
| PLE/5 | PLE/6 | PLE/7 | PLE/8 |
| • Processes 2½ lbs. per hr. and 20 lbs. in 8 hrs | • Processes 3 lbs. per hr. and 24 lbs. in 8 hrs. | • Processes 3½ lbs. per hr. and 28 lbs. in 8 hrs | • Processes 4 lb. per hr. and 32 lbs. in 8 hrs. |
| • Good for Intermediate Operations or mobile applications | • Good for Intermediate Operations or mobile applications | • Good for Larger Operations | • Good for Larger Operations |
| • Economic Cost Business level | • Economic Cost Business level | • Economic Cost Business level | • Economic Cost Business level |
| • Fully Automated | • Fully Automated | • Fully Automated | • Fully Automated |
| • Smallest footprint (fits on a counter-top) | • Smallest footprint (fits on a counter-top) | • Moderate footprint (fits on a portable cart) | • Moderate footprint (fits on a portable cart) |
| • Runs on 110V 20 amp circuit | • Runs on 110V 20 amp circuit | • Runs on 110V 20 amp circuit | • Runs on 110V 20 amp circuit |
| • Dimensions: 49” W X 26” H X 18” D | • Dimensions: 57” W X 26” H X 18” D | • Dimensions: 65” W X 26” H X 18” D | • Dimensions: 73” W X 26” H X 18” D |
Consumables
| Part # | Description |
| PLE-CAR-SS05 | 5ml stainless steel PLE cartridge |
| PLE-CAR-SS10 | 10ml stainless steel PLE cartridge |
| PLE-CAR-SS100 | 100ml stainless steel PLE cartridge |
| PLE-CAR-SS20 | 20ml stainless steel PLE cartridge |
| PLE-CAR-SS40 | 40ml stainless steel PLE cartridge |
| PLE-CAR-SS200 | 200ml Stainless Steel Cartridge |
TurboTrace ABN
TurboTrace® ABN SPE System: Fully Automated Multi-Cartridge Sample Preparation system
The TurboTrace® ABN SPE System is a fully automated, multi-cartridge, multi-fractionation solution capable of processing up to six samples simultaneously. It supports any solid-phase extraction (SPE) method requiring multiple cartridges or fractions, making it ideal for laboratories aiming to enhance workflow efficiency and productivity.
Key Features of the TurboTrace® ABN SPE System
- Simultaneous Processing: Runs up to six samples at once, significantly increasing throughput.
- Multi-Cartridge Compatibility: Handles SPE methods involving multiple cartridges or fractions with ease.
- Total Automation: Automates complex manual processes, minimizing hands-on time and reducing errors.
- Integrated Drying and Concentration: Combines extraction, drying, and concentration into a single streamlined step.
Applications of the TurboTrace® ABN SPE System
The TurboTrace® ABN SPE System automates existing manual techniques for advanced laboratory workflows. It is designed for use with ABN methods, including EPA Methods 625 and 8270D, which analyze semi-volatile compounds in a variety of matrices.
Challenges Addressed by the TurboTrace® ABN SPE System:
- Complex Compound Groups: Methods often include phenols, anilines, PAHs, phthalates, explosives, pesticides, and n-nitrosoamines, requiring tedious liquid-liquid extractions (LLE) with multiple pH adjustments.
- High Elution Volumes: Large elution volumes (>360 mL of methylene chloride) can lead to low recoveries and poor analytical precision.
- Manual Steps: The need for multiple manual steps increases the potential for human error and contamination.
How It Works
- Sample Loading: Samples are loaded onto the SPE cartridge using vacuum or positive pressure.
- Drying Step: Automated nitrogen drying replaces manual drying techniques, enhancing consistency and reducing errors.
- Fractionation: The system automatically fractionates analytes into acid and base fractions.
- Elution and Concentration: The analytes are eluted directly into the SuperVap® Concentrator, where they are concentrated to the final volume in an autosampler vial, ready for analysis.
This fully closed system ensures the lowest background levels, delivering reproducible and consistent results every time.
Benefits of Using the TurboTrace® ABN SPE System
- Streamlined Workflow: Automates every step from extraction to concentration, saving valuable time.
- Improved Accuracy: Reduces the risk of human error and contamination, ensuring reliable results.
- Enhanced Productivity: Processes multiple samples simultaneously, making it ideal for high-throughput laboratories.
- High-Quality Results: Delivers precise fractionation and consistent analyte recovery.
Why Choose TurboTrace® ABN SPE System?
The TurboTrace® ABN SPE System revolutionizes laboratory sample preparation by automating time-consuming, error-prone steps. Its advanced design integrates key processes, reduces solvent usage, and improves analyte recovery. For laboratories adhering to EPA Methods or handling complex analyte mixtures, the TurboTrace® ABN SPE System is the ultimate solution for achieving faster, more accurate, and reproducible results
Product Video
Details
The TurboTrace® ABN SPE system is the only SPE system that combines Dual Cartridge extraction and fractionation, drying and concentration into one step — providing a truly automated total sample prep solution for the laboratory. Simply load samples onto the TurboTrace ABN SPE system to trigger the automated extraction process. After loading the sample onto the SPE cartridge, the drying step is accomplished using Nitrogen. This drying step replaces manual techniques. The analytes of interest are then eluted directly to the SuperVap Concentrator where the concentration process automatically brings the extract to final volume and places it directly into an autosampler vial, ready for final analysis. Automating these processes into one step ensures the highest quality results in the shortest amount of time and eliminates both human error and the possibility of contamination. The fullprocess is complete in just over 1 hour versus 16 to 18 hrs and cuts the solvent consumption by 70%.
The TurboTrace ABN SPE system uses positive pressure pumping for precise and accurate delivery of conditioning, washing and elution solvents. The TurboTrace ABN SPE system is specifically designed to isolate analytes of interest from a wide variety of liquid matrices such as urine, blood, water, milk, beverages. Sample sizes range from 2 mL to 8 L and use the same bottle the sample was collected in. Sample loading rates are programmable. A vacuum or positive pressure pump is used to load samples onto the SPE cartridges and columns at unprecedented speeds and it easily handles both clean and tough sample matrices. The TurboTrace ABN SPE system concentrates samples up to 250 mL directly to a GC vial. The Sample Processing Module is designed to use all standard formats of SPE cartridges and columns on the market today. For guaranteed results, especially when dealing with low limits of detection, we recommend FMS prepacked columns and cartridges. Sample Processing Modules can be easily swapped out to perform cleanup column chemistries allowing the lab to multipurpose the TurboTrace ABN SPE system to automate other sample prep processes.
The TurboTrace ABN SPE system is a Multi Cartridge, Multi fractionation system that can be used for any SPE method requiring more than one cartridge or fraction.
Reduces Errors
One-step automated SPE and concentration eliminates human error, saves labor costs and reduces solvent usage while increasing your sample throughput
Fully Automated
Hyphenates the entire sample prep process–extraction, drying and concentration steps–into a one step program.
Runs up to 8 samples, simultaneously
Sample Liquid Level Sensor to detect when the Sample has finished loading Automatic Sample bottle rinse
Concentrates samples up to 250 mL directly to a GC vial
Waste liquid level sensor to prevent waste overflow
Dual Cartridge extraction and fractionation of Acid/Base/Neutral
High Speed
The fastest automated sample processing available for ABN methods using SPE cartridges and columns ready for analysis in hours versus days
Run up to eight samples simultaneously
Vacuum for fast loading of large volume samples
Versatile
Handles a wide range of sample sizes and all matrix types
Dual Cartridge allows for many other types of multi cartridge applications
Up to 3 fractions per run
Sample Sizes 2 mL to many liters
Sample Liquid Level Sensor to detect when the Sample has finished loading
Expandable from 1 to 8 modules
Efficient
Uses all SPE cartridge and column sizes
Positive pressure pumping for loading small volume samples
Nitrogen drying
Compliant
Complies with existing methods that require vacuum, positive pressure pumping for the precise delivery of sample and solvents
Dispenses up to six solvents using an HPLC pump to deliver precise volumes and flow rates for conditioning and elution
Easy Documentation
Programs and stores an unlimited number of methods and runs on an SD Card Easy method transfer
Easy-to-use software
Specifications
Dimensions:
15”W x 18”D x 35”H
15”W x 18”D x 35”H
Weight:
65lbs
Gas Requirements:
Nitrogen – 20PSI minimum
Vacuum Requirements:
25”Hg minimum
Pump:
Piston Displacement
Flow rate:
0.2 to 15ml/minute
Electrical Input:
110/220 Volts, 50/60HZ
Controller:
Integrated Touch Screen Control
Consumables
| Part number | Description |
| ABN-CAR-CH | ABN Charcoal Cartridge |
| ABN-CAR-ONG | ABN Oil & Grease Cartridge |
| ABN-CAR-EX | ABN Exchange Cartridge |
| SPE-ADP-1 | SPE 1ml Cartridge Adapter |
| SPE-ADP-20 | SPE 20ml Cartridge Adapter |
| SPE-ADP-3 | SPE 3ml Cartridge Adapter |
| SPE-ADP-6 | SPE 6ml Cartridge Adapter |
| SPE-BT.5L | SPE Sample Bottle 500ml |
| SPE-BT1 | SPE Sample Bottle 1L |
| SPE-BT1.25L | SPE Sample Bottle 1250ml |
| SPE-BTRC | SPE Sample Bottle Rinse Cap |
| SPE-CAP-1L | SPE Bottle Cap with Loading and Sample Rinse Tubings and Adapters, 1L |
| SPE-CAP-2L | SPE Bottle Cap with Loading and Sample Rinse Tubings and Adapters, 2L |
| SPE-CAR1-C18 | SPE Cartridge 1 gram C18 |
| SPE-CAR1-DVB | SPE Cartridge 1 gram DVB |
| SPE-CAR5-C18 | SPE Cartridge 5 gram C18 |
| SPE-CAR6-DVB | SPE Cartridge 6 gram DVB |
TurboTrace PFC
Solid Phase Extraction of PFAS with the TurboTrace PFC SPE System
The TurboTrace PFC SPE system is a fully automated sample preparation system designed for the solid phase extraction of PFAS and other perfluorinated compounds from wastewater. This system runs up to 8 samples simultaneously, delivering consistent, reproducible results while eliminating the need for sample reruns.
As a closed system, it incorporates a vacuum or positive pressure pump to load samples in compliance with all SPE methods, ensuring high efficiency in the solid phase extraction of PFAS. The system uses precise positive pressure pumping to condition, wash, and elute solvents accurately. It is engineered to isolate analytes from various solid and liquid matrices, including urine, blood, water, milk, beverages, meat, soil, and more.
Sample sizes range from 2 mL to unlimited and can be processed directly from the original collection bottle. With programmable sample loading rates, the TurboTrace PFC SPE system easily handles both clean and harsh sample matrices. The integrated liquid sensor detects when samples are fully loaded, triggering the next automated steps.
The Sample Processing Module supports all standard formats of SPE cartridges available today. For guaranteed results, especially with low detection limits, FMS recommends using our prepacked cartridges, which are specifically designed for the solid phase extraction of PFAS.
Applications:
Drinking Water
Waste Water
Blood
Milk and Beverages
Method:
Consistent, Low Background, Reproducible Automated Extraction of Perfluorakylated Substances
Applications
Details
The TurboTrace PFC (Perfluoralkylated substances) SPE system is designed to streamline your laboratory’s workflow and increase productivity by automating the manual steps in your sample preparation process. It is designed for high throughput and tough sample matrices. The TurboTrace PFC SPE system automates existing manual SPE techniques and replaces older manual Liquid-Liquid Extraction techniques and outdated semi-automated instruments. Perfluoralkylated substances is a general term used to describe substances which are largely comprised of or contain a perfluorinated or polyfluorinated carbon chain moiety such as F(CF2)n- or F(CF2)n-(C2H4)n. In recent years, there has been increasing concern over the levels of perfluorinated and polyfluorinated chemicals, such as PFOS (perfluorosulfonate) and PFOA (perfluorooctanoicacid), in the global environment and their fate and possible adverse effects in the environment. PFOS is now subject to varying but increasing levels of control in a number of countries. The TurboTrace PFC SPE system, the first automated solid phase extraction system made specifically for PFC extraction and concentration. Primarily effective at reducing background contamination, extraction and concentration of aqueous samples takes less than two hours
Reduces Errors
One-step automated SPE and concentration eliminates human error, saves labor costs and reduces solvent usage while increasing your sample throughput
Fully Automated
Hyphenates the entire sample prep process–extraction, drying and concentration steps–into a one step program.
Runs up to 8 samples simultaneously
Sample Liquid Level Sensor to detect when the Sample has finished loading
Automatic Sample bottle rinse
Concentrates samples up to 250 mL directly to a GC vial
High Speed
The fastest automated sample processing available for SPE cartridges and columns
Run up to eight samples simultaneously
Vacuum for fast loading of large volume samples
Versatile
Handles a wide range of sample sizes and all matrix types
Sample Sizes 2 mL to many liters
Sample Liquid Level Sensor to detect when the Sample has finished loading
Expandable from 1 to 8 modules
Efficient
Uses all SPE cartridge and column sizes
Positive pressure pumping for loading small volume samples
Nitrogen drying
Compliant
Complies with existing methods that require vacuum, positive pressure pumping for the precise delivery of sample and solvents
Dispenses up to six solvents using an HPLC pump to deliver precise volumes and flow rates for conditioning and elution
Easy Documentation
Programs and stores an unlimited number of methods and runs on an SD Card Easy method transfer
Easy-to-use software
Specifications
Dimensions:
15”W x 18”D x 28”H
Weight:
65lbs.
Gas Requirements:
Nitrogen – 20 PSI minimum
Pump:
Piston Displacement Flow
Flow rate: 0.2 to 15ml/minute
Vacuum -25 Hg
Electrical Input:
110/220Volts, 50/60HZ
Controller:
Integrated Touch Screen Control
Consumables
| Part number | Description |
| SPE-ADP-1 | SPE 1ml Cartridge Adapter |
| SPE-ADP-20 | SPE 20ml Cartridge Adapter |
| SPE-ADP-3 | SPE 3ml Cartridge Adapter |
| SPE-ADP-6 | SPE 6ml Cartridge Adapter |
| SPE-BT.5L | SPE Sample Bottle 500ml |
| SPE-BT1 | SPE Sample Bottle 1L |
| SPE-BT1.25L | SPE Sample Bottle 1250ml |
| SPE-BTRC | SPE Sample Bottle Rinse Cap |
| SPE-CAP-1L | SPE Bottle Cap with Loading and Sample Rinse Tubings and Adapters, 1L |
| SPE-CAP-2L | SPE Bottle Cap with Loading and Sample Rinse Tubings and Adapters, 2L |
| SPE-CAR1-C18 | SPE Cartridge 1 gram C18 |
| SPE-CAR1-DVB | SPE Cartridge 1 gram DVB |
| SPE-CAR5-C18 | SPE Cartridge 5 gram C18 |
| SPE-CAR6-DVB | SPE Cartridge 6 gram DVB |
TurboTrace Parallel SPE
TurboTrace® Parallel Solid Phase Extraction System: High-Throughput Parallel SPE System
The TurboTrace® Parallel SPE System is an advanced Solid Phase Extraction System designed to streamline laboratory workflows and boost productivity. It automates manual solid-phase extraction (SPE) techniques, replacing outdated liquid-liquid extraction methods and semi-automated instruments. Built for high throughput and tough sample matrices, the TurboTrace Parallel SPE System is ideal for laboratories seeking precision and efficiency.
Key Features of the TurboTrace® Parallel SPE System
- Simultaneous Processing: Automatically processes up to six samples simultaneously, saving time and increasing productivity.
- Versatile Sample Handling: Compatible with a wide variety of liquid matrices, including urine, blood, water, milk, and beverages.
- Flexible Sample Sizes: Handles sample volumes from 2 mL to unlimited, using the same bottle the sample was collected in.
- Programmable Operations: Offers customizable solvent conditioning, washing, and elution rates.
- Precise Delivery: Utilizes positive pressure pumping for accurate solvent delivery and superior performance with all SPE methods.
- Automation: Incorporates vacuum or positive pressure pumps for efficient sample loading and transitions automatically to subsequent steps with a built-in liquid sensor.
- Concentration Capability: Concentrates up to 250 mL directly into a GC vial for analysis.
Applications of the TurboTrace® Parallel SPE System
This system is specifically designed to isolate analytes of interest from a wide range of liquid matrices. It is ideal for use in the following applications:
- Drinking Water Analysis
- Wastewater Analysis
- Blood Testing
- Milk and Beverage Testing
How It Works
- Sample Loading: The system uses vacuum or positive pressure to load samples quickly, regardless of matrix complexity.
- Solvent Conditioning and Washing: Positive pressure pumps ensure precise delivery of conditioning, washing, and elution solvents.
- Automated Transitions: A built-in liquid sensor detects when the sample is loaded and triggers the next steps automatically.
- Sample Concentration: Samples up to 250 mL are concentrated directly into GC vials for analysis.
The system’s Sample Processing Module supports all standard formats of SPE cartridges available on the market. For optimal results, especially for low limits of detection, FMS prepacked cartridges are recommended.
Benefits of the TurboTrace® Parallel SPE System
- Efficiency: Processes multiple samples simultaneously, making it ideal for high-throughput laboratories.
- Accuracy: Delivers precise and reproducible results, even for tough sample matrices.
- Convenience: Eliminates manual steps, reduces human error, and ensures faster sample preparation.
- Flexibility: Handles diverse sample types and volumes with ease, streamlining laboratory workflows.
Why Choose the TurboTrace® Parallel SPE System?
The TurboTrace® Parallel SPE System combines advanced automation, high precision, and flexibility to meet the demands of modern laboratories. Whether analyzing drinking water, wastewater, blood, or beverages, this system simplifies complex workflows, reduces turnaround time, and delivers consistent, high-quality results.
Supports EPA Methods
EPA Method 506 Phthalates and Adipate Esters
EPA Method 508.1 Chlorinated Pesticides, Herbicides, and Organohalides
EPA Method 515.2 Chlorinated Acids
EPA Method 521 Nitrosamines
EPA Method 525.2 Semi-volatiles
EPA Method 526 Semi-volatiles
EPA Method 527 Selected Pesticides and Flame Retardants
EPA Method 528 Phenols
EPA Method 529 Explosives
EPA Method 532 Phenylurea Compounds
EPA Method 535 Chloroacetanilide and other Acetamide Herbicides
EPA Method 548.1 Endothall
EPA Method 549.2 Diquat and Paraquat
EPA Method 550.1 PAH’s
EPA Method 552.1 Haloacetic Acids and Dalapon
EPA Method 553 Benzidines and Nitrogen Containing Pesticides
EPA Method 608 Chlorinated Pesticides and PCB’s
EPA Method 1613 Dioxin
EPA Method 1664A Oil and Grease and SGT-HEM
EPA Method 1668A Toxic PCB’s by Isotope Dilution and GC/MS
EPA Method 1694 Pharmaceutical and Personal Care Products
EPA Method 8061 Phthalate esters
EPA Method 8081 TCLP Organochlorine pesticides
EPA Method 8082 PCB’s
EPA Method 8095 Explosives
EPA Method 8141 Organophosphorus pesticides
EPA Method 8321 TCLP Phenoxyacid herbicides
EPA Method 8330 Nitroaromatics / Nitramines
EPA Method 508.1 Chlorinated Pesticides, Herbicides, and Organohalides
EPA Method 515.2 Chlorinated Acids
EPA Method 521 Nitrosamines
EPA Method 525.2 Semi-volatiles
EPA Method 526 Semi-volatiles
EPA Method 527 Selected Pesticides and Flame Retardants
EPA Method 528 Phenols
EPA Method 529 Explosives
EPA Method 532 Phenylurea Compounds
EPA Method 535 Chloroacetanilide and other Acetamide Herbicides
EPA Method 548.1 Endothall
EPA Method 549.2 Diquat and Paraquat
EPA Method 550.1 PAH’s
EPA Method 552.1 Haloacetic Acids and Dalapon
EPA Method 553 Benzidines and Nitrogen Containing Pesticides
EPA Method 608 Chlorinated Pesticides and PCB’s
EPA Method 1613 Dioxin
EPA Method 1664A Oil and Grease and SGT-HEM
EPA Method 1668A Toxic PCB’s by Isotope Dilution and GC/MS
EPA Method 1694 Pharmaceutical and Personal Care Products
EPA Method 8061 Phthalate esters
EPA Method 8081 TCLP Organochlorine pesticides
EPA Method 8082 PCB’s
EPA Method 8095 Explosives
EPA Method 8141 Organophosphorus pesticides
EPA Method 8321 TCLP Phenoxyacid herbicides
EPA Method 8330 Nitroaromatics / Nitramines
Applications
Extraction of Phosphorus Flame Retardants in Drinking Water by TurboTrace
EPA 1664A Oil and Grease by Solid Phase Extraction
EPA 8270 Automated SPE and Concentration for an MDL study in Water Using SIM by TurboTrace
EPA 632 Carbamate and Urea Pesticides in Waste Water by TurboTrace
EPA 607 Nitrosamines in Waste Water by TurboTrace
EPA 604 Phenols in Wastewater by TurboTrace
EPA 554 Carbonyl Compounds in Drinking Water by TurboTrace
EPA 553 Benzidines and Nitrogenous Pesticides in Drinking Water by TurboTrace
EPA 552.1 Haloacetic Acids Dalapon in Drinking Water by TurboTrace
EPA 550.1 Polycylic Aromatic Hydrocarbons in Drinking Water by TurboTrace
EPA 549.2 Diquat and Paraquat in Drinking Water by TurboTrace
EPA 548.1 Endothall in Drinking Water by TurboTrace
EPA 535 Acetanilide and other Herbicide Degradates in Drinking Water by TurboTrace
EPA 532 Phenylurea Compounds in Drinking Water by TurboTrace
EPA 529 Explosives in Drinking Water by Solid Phase Extraction
EPA 528 Phenols in Drinking Water by TurboTrace
EPA 525.2 Automated Solid Phase Extraction Semi Volatile Organic Compounds in Drinking Water
EPA 522 Analysis of 1-4-Dioxane in Drinking Water
EPA 508 Organochlorine Pesticides in Drinking Water with Automated SPE
Dioxin in Drinking Water by One Step Solid Phase Extraction
Automated Solid Phase Extraction (SPE) of Organochlorine Pesticides in Water
Automated One Step SPE and Concentration of Nitrogen and Phosphorus Containing Pesticides in Water
Automated One Step Solid Phase Extraction and Concentration of PCBs in Drinking Water
Details
The TurboTrace Parallel SPE system combines extraction, drying and concentration into one step — providing a truly automated total sample prep solution for the laboratory. Simply load samples onto the TurboTrace Parallel SPE system, use the touch screen to trigger the automated extraction process. Load the sample onto the SPE cartridge using Vacuum or Positive Pressure Pumping, the drying step is accomplished using vacuum or nitrogen or both. This drying step replaces manual techniques such as sodium sulfate drying. The analytes of interest are then eluted directly to the SuperVap Concentrator where the concentration process automatically brings the extract to final volume in a autosampler vial, ready for final analysis. Automating these processes into one step ensures the highest quality results in the shortest amount of time and eliminates both human error and the possibility of contamination.
The TurboTrace Parallel SPE system incorporates vacuum or positive pressure pump to load samples for compliance with all SPE methods. It uses positive pressure pumping for precise and accurate delivery of conditioning, washing and elution solvents. The TurboTrace Parallel SPE system is specifically designed to isolate analytes of interest from a wide variety of liquid matrices such as urine, blood, water, milk, beverages. Sample sizes range from 2 mL to 8 L and use the same bottle the sample was collected in. Sample loading rates are programmable. A vacuum or positive pressure pump is used to load samples onto the SPE cartridges and columns at unprecedented speeds and it easily handles both clean and tough sample matrices. An liquid sensor detects when the sample has been loaded, triggering the system to initate next steps. The TurboTrace Parallel SPE system concentrates samples up to 250 mL directly to a GC vial. The Sample Processing Module is designed to use all standard formats of SPE cartridges and columns on the market today. For guaranteed results, especially when dealing with low limits of detection, we recommend FMS prepacked columns and cartridges. Sample Processing Modules can be easily swapped out to perform cleanup column chemistries allowing the lab to multipurpose the TurboTrace Parallel SPE system to automate other sample prep processes.
Reduces Errors
One-step automated SPE and concentration eliminates human error, saves labor costs and reduces solvent usage while increasing your sample throughput
Fully Automated
Hyphenates the entire sample prep process–extraction, drying and concentration steps–into a one step program.
Runs up to 8 samples simultaneously
Sample Liquid Level Sensor to detect when the Sample has finished loading
Automatic Sample bottle rinse
Concentrates samples up to 250 mL directly to a GC vial
High Speed
The fastest automated sample processing available for SPE cartridges and columns
Run up to eight samples simultaneously
Vacuum for fast loading of large volume samples
Versatile
Handles a wide range of sample sizes and all matrix types
Sample Sizes 2 mL to many liters
Sample Liquid Level Sensor to detect when the Sample has finished loading
Expandable from 1 to 8 modules
Efficient
Uses all SPE cartridge and column sizes
Positive pressure pumping for loading small volume samples
Nitrogen drying
Compliant
Complies with existing methods that require vacuum, positive pressure pumping for the precise delivery of sample and solvents
Dispenses up to six solvents using an HPLC pump to deliver precise volumes and flow rates for conditioning and elution
Easy Documentation
Programs and stores an unlimited number of methods and runs on an SD Card Easy method transfer
Easy-to-use software
Specifications
Specifications
Dimensions:
15”W x 18”D x 28”H
Weight:
65lbs.
Gas Requirements:
Nitrogen – 20 PSI minimum
Pump:
Piston Displacement Flow
Flow rate: 0.2 to 15ml/minute
Vacuum -25 Hg
Electrical Input:
110/220Volts, 50/60HZ
Controller:
Integrated Touch Screen Control
Consumables
| Part number | Description |
| SPE-ADP-1 | SPE 1ml Cartridge Adapter |
| SPE-ADP-20 | SPE 20ml Cartridge Adapter |
| SPE-ADP-3 | SPE 3ml Cartridge Adapter |
| SPE-ADP-6 | SPE 6ml Cartridge Adapter |
| SPE-BT.5L | SPE Sample Bottle 500ml |
| SPE-BT1 | SPE Sample Bottle 1L |
| SPE-BT1.25L | SPE Sample Bottle 1250ml |
| SPE-BTRC | SPE Sample Bottle Rinse Cap |
| SPE-CAP-1L | SPE Bottle Cap with Loading and Sample Rinse Tubings and Adapters, 1L |
| SPE-CAP-2L | SPE Bottle Cap with Loading and Sample Rinse Tubings and Adapters, 2L |
| SPE-CAR1-C18 | SPE Cartridge 1 gram C18 |
| SPE-CAR1-DVB | SPE Cartridge 1 gram DVB |
| SPE-CAR5-C18 | SPE Cartridge 5 gram C18 |
| SPE-CAR6-DVB | SPE Cartridge 6 gram DVB |
TurboTrace Sequential Parallel SPE
An Overview of Solid Phase Extraction (SPE)
Solid Phase Extraction (SPE) is a widely used sample preparation method that separates analytes from complex solutions using a solid and a liquid phase. This method is typically employed to clean up samples before chromatographic or other analytical techniques quantify the analytes.
Key Features and Workflow of Solid Phase Extraction
The general SPE procedure involves three main steps:
- Sample Loading: The solution containing the analyte is loaded onto the stationary phase.
- Washing: Undesired components are washed away, leaving the analytes bound to the stationary phase.
- Elution: The desired analytes are eluted with a suitable solvent into a collection tube.
SPE instruments utilize stationary phases similar to those in liquid chromatography columns. The stationary phase, housed in glass or plastic columns, sits above a frit or glass wool. These columns may also include a top frit and a stopcock to control solvent flow.
Cartridge Design and Usage:
Commercial SPE cartridges range in size from 1 to 60 mL and are single-use. A vacuum manifold or positive pressure pump is often employed to increase solvent flow rates through the cartridge. The liquid that passes through is collected in a tube positioned below the SPE cartridge.
Applications of Solid Phase Extraction
SPE is versatile and effective for numerous sample matrices, including:
- Water and Beverages
- Serum and Urine
- Milk and Food Products
- Pharmaceuticals
Addressing Complex Sample Matrices
Some sample matrices, like those found in pharmaceuticals or environmental samples, contain multiple interferences that complicate analyte detection. SPE effectively removes these interferences, improving target compound quantification and preventing analytical instrument contamination.
Additionally, SPE can serve as a fractionation tool, separating a wide range of compounds from a single sample. For instance:
- Hydrocarbon Analysis: SPE can isolate aliphatic and aromatic hydrocarbons from petroleum hydrocarbon samples, allowing dual analysis from one sample.
- Trace-Level Concentration: SPE concentrates trace-level compounds of interest by passing large volumes of the sample matrix through the cartridge, followed by elution.
Challenges in Manual SPE and FMS’s Automated Solutions
While SPE is a powerful tool, traditional manual procedures are labor-intensive and prone to human error. Manual extractions often require numerous sequential steps, increasing the risk of inconsistent results.
FMS’s Automated SPE Systems
FMS, Inc. addresses these challenges by designing advanced instruments that automate SPE processes. These systems combine multiple steps—extraction, drying, and concentration—into a single, unattended operation. Benefits include:
- Reduced Labor: Automated workflows eliminate the need for manual intervention.
- Enhanced Accuracy: Automation minimizes human error, ensuring consistent results.
- Improved Efficiency: Fully hyphenated systems reduce processing time and increase throughput.
Benefits of SPE Automation
- Improved Reproducibility: Automation ensures consistent results across samples.
- Time Savings: Processes run unattended, freeing up laboratory staff for other tasks.
- Cleaner Analysis: Automated SPE systems minimize contamination and reduce analytical instrument maintenance.
- Streamlined Workflows: Combines multiple sample prep steps into one, simplifying complex procedures.
Why Choose Automated SPE Solutions?
Solid Phase Extraction remains an essential technique for laboratories handling complex matrices. By leveraging FMS’s automated SPE systems, laboratories can overcome the challenges of manual workflows, achieve better reproducibility, and enhance productivity. Whether analyzing trace compounds in environmental samples or fractionating hydrocarbons, automated SPE ensures superior results with minimal effort.
EPA Methods
EPA Methods:
500 Series
600 Series
1600 Series
8000 Series
500 Series
600 Series
1600 Series
8000 Series
Details
TurboTrace® Sequential Parallel Automated Solid Phase Extraction System
TThe TurboTrace Sequential Parallel Automated Solid Phase Extraction System is a One-Step Extraction and Concentration System is designed to streamline your laboratory’s workflow and increase productivity by automating the manual steps in your sample preparation process. The TurboTrace Sequential Parallel Automated Solid Phase Extraction System automates existing manual SPE techniques and replaces older manual Liquid-Liquid Extraction techniques and outdated semi-automated instruments.
The TurboTrace Sequential Parallel Automated Solid Phase Extraction System is the only SPE system that combines extraction, drying and concentration into one step — providing a truly automated total sample prep solution for the laboratory. Simply load samples onto the PowerPrep SPE system to trigger the automated extraction process. After loading the sample onto the SPE cartridge, the drying step is accomplished using Nitrogen. This drying step replaces manual techniques. The analytes of interest are then eluted directly to the SuperVap Concentrator where the concentration process automatically brings the extract to final volume and places it directly into an autosampler vial, ready for final analysis. Automating these processes into one step ensures the highest quality results in the shortest amount of time and eliminates both human error and the possibility of contamination.
The TurboTrace Sequential Parallel Automated Solid Phase Extraction System uses positive pressure pumping for precise and accurate delivery of conditioning, washing and elution solvents. The TurboTrace Sequential Parallel Automated Solid Phase Extraction System is specifically designed to isolate analytes of interest from a wide variety of liquid matrices such as urine, blood, water, milk, beverages. Sample sizes range from 2 mL to 8 L and use the same bottle the sample was collected in. Sample loading rates are programmable. A vacuum or positive pressure pump is used to load samples onto the SPE cartridges and columns at unprecedented speeds and it easily handles both clean and tough sample matrices. The TurboTrace Sequential Parallel Automated Solid Phase Extraction System concentrates samples up to 250 mL directly to a GC vial. The Sample Processing Module is designed to use all standard formats of SPE cartridges and columns on the market today. For guaranteed results, especially when dealing with low limits of detection, we recommend FMS prepacked columns and cartridges. Sample Processing Modules can be easily swapped out to perform cleanup column chemistries allowing the lab to multipurpose the PowerPrep to automate other sample prep processes.
Reduces Errors
One-step automated SPE and concentration eliminates human error, saves labor costs and reduces solvent usage while increasing your sample throughput
Fully Automated
Hyphenates the entire sample prep process–extraction, drying and concentration steps–into a one step program.
Runs up to five different methods/sample matrices sequentially
Concentrates samples up to 250 mL directly to a GC vial.
Automatic Sample bottle rinse
High Speed
The fastest automated sample processing available for SPE cartridges and columns
Run up to six samples simultaneously, up to 30 samples total
Vacuum for fast loading of large volume samples
Versatile
Handles a wide range of sample sizes and all matrix types
Sample Sizes 2 mL to 8 L
Expandable from 1 to 6 modules
Efficient
Uses all SPE cartridge and column sizes
Positive pressure pumping for loading small volume samples
Nitrogen drying
Compliant
Complies with existing methods that require vacuum, positive pressure pumping for the precise delivery of sample and solvents
Dispenses up to six solvents using an HPLC pump to deliver precise volumes and flow rates for conditioning and elution
Easy Documentation
Programs and stores an unlimited number of methods and runs
Easy-to-use software
Specifications
TurboTrace Sequential Parallel SPE
Dimensions: 15” W x 18” D x 35” H
Weight: 130 lbs.
Gas Requirements: Nitrogen – 20 PSI minimum
Vacuum Requirements: 25” Hg minimum
Pump: Piston Displacement
Flow rate: 0.2 to 15 mL/minute
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: PC based
SuperVapVap Concentration System
Dimensions:7” W x 13” D x 12” H
Weight: 20 lbs.
Gas Requirements: Nitrogen – 20 PSI minimum
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: PC based
Bath: Dry
Consumables
| Part number | Description |
| SPE-ADP-1 | SPE 1ml Cartridge Adapter |
| SPE-ADP-20 | SPE 20ml Cartridge Adapter |
| SPE-ADP-3 | SPE 3ml Cartridge Adapter |
| SPE-ADP-6 | SPE 6ml Cartridge Adapter |
| SPE-BT.5L | SPE Sample Bottle 500ml |
| SPE-BT1 | SPE Sample Bottle 1L |
| SPE-BT1.25L | SPE Sample Bottle 1250ml |
| SPE-BTRC | SPE Sample Bottle Rinse Cap |
| SPE-CAP-1L | SPE Bottle Cap with Loading and Sample Rinse Tubings and Adapters, 1L |
| SPE-CAP-2L | SPE Bottle Cap with Loading and Sample Rinse Tubings and Adapters, 2L |
| SPE-CAR1-C18 | SPE Cartridge 1 gram C18 |
| SPE-CAR1-DVB | SPE Cartridge 1 gram DVB |
| SPE-CAR5-C18 | SPE Cartridge 5 gram C18 |
| SPE-CAR6-DVB | SPE Cartridge 6 gram DVB |
TurboTrace® PFC Sequential Parallel SPE
Automated Solid Phase Extraction System for PFAS/PFOS in Water
Revolutionizing PFAS Analysis with the TurboTrace PFC SPE System
The TurboTrace PFC Parallel Sequential Automated Solid Phase Extraction System is a cutting-edge, one-step solution for the solid phase extraction of PFAS and PFOS in drinking water and wastewater. Designed to simplify your laboratory workflow, it eliminates manual steps in the sample preparation process, significantly boosting productivity.
Streamlined Automation for Modern Labs
This system automates existing manual SPE techniques and replaces outdated extraction methods and instruments. By integrating advanced features, the TurboTrace PFC SPE System ensures consistent, reproducible results and minimizes errors commonly associated with manual processes.
Key Features of the TurboTrace PFC SPE System
- Parallel Sequential Design: Processes multiple samples efficiently while maintaining sequential precision.
- One-Step Extraction and Concentration: Combines the extraction and concentration processes into a single automated workflow.
- Compatibility: Supports all standard SPE cartridges, ensuring flexibility for a variety of sample types.
- Enhanced Productivity: Reduces manual labor and frees up valuable time for lab technicians.
Applications and Benefits
The TurboTrace PFC SPE System is ideal for laboratories analyzing PFAS/PFOS in water matrices, such as drinking water and wastewater. It replaces older, manual methods with a reliable, automated solution that increases throughput and ensures compliance with regulatory requirements.
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· Closed System once the sample bottle is attached the system is never exposed to the outside laboratory, Eliminating Background Contamination. · Programmable Positive Pressure pumping for solvent selection, flow rates, conditioning, washing, eluting, and loading samples to produce consistent, reproducible results. · Automatic Programmable Sample Bottle rinse and loading · Solvent mixing · Up to five solvents · Vacuum pump for high-speed sample loading of clean or dirty particulate laden samples · Vacuum Cartridge Drying · Nitrogen Cartridge Drying |
· Components are Delrin™, Peek™, Stainless steel, LLDPE, Medical Grade PP, HDPE · Modular and scalable Run 1 to 6 samples simultaneously, up to a total of 30 samples sequentially · Runs up to 5 different methods/sample matrices sequentially · Sample Sizes from 2ml to unlimited · Uses sample bottle caps from your lab, no custom bottle caps or adapters required. |
· Designed to use all SPE cartridges formats/sizes · Separates Aqueous and Organic Waste · Waste overflow alarm · Graphical display for each SPE step · Touchscreen display for operating the system · Deliver extracts automatically and directly to the SuperVap PFC 24 Concentrator for final blow down into a 15ml Centrifuge tube |
EPA Methods
Supports EPA and other Methods
EPA Method 533
Determination Of Per- And Polyfluoroalkyl Substances In Drinking Water By Isotope
Dilution Anion Exchange Solid Phase Extraction
EPA Method 537.1
Determination of Selected Per- and Polyfluorinated
Alkyl Substances in Drinking Water by Solid Phase Extraction
EPA 8327 with 3512
PFAS in drinking, surface, wastewater 24 compounds; no SPE; mixing 1:1 with solvent and add standards (isotope dilution) filtration; LC/MS/MS
ASTM 7968
21 PFAS sand and soil, solvent extraction and filtration, LC/MS
EPA Method 1694
Pharmaceutical and Personal Care Products
EPA Method 1694
Pharmaceutical and Personal Care Products
Details
Benefits of TurboTrace PFC Parallel Sequential Automated Solid Phase Extraction:
REDUCES ERRORS
- One step automated SPE and concentration eliminates human error, saves labor costs and reduces solvent usage while increasing your sample throughput
- Put the sample on the system and get the final extract automatically delivered and concentrated, ready to analyze on the LC/MS eliminating the majority of human intervention
COMPLIANT
- Complies with existing methods that require vacuum, positive pressure pumping for the precise delivery of sample and solvent
- Dispenses up to five solvents using an HPLC pump to deliver precise volumes and flow rates for conditioning, elution and bottle rinse.
FULLY AUTOMATED
EASY DOCUMENTATION
- Programs and stores an unlimited number of methods and runs on an SD card
- Hyphenates the entire sample prep process: extraction, drying and concentration step into a One-Step Sample Prep workflow
- Transfer Methods to LIMS
EASY-TO-USE SOFTWARE
- Graphical SPE step indicator icons keep users informed
- Runs up to five different methods/sample matrices sequentially
- Concentrates Extractions delivered directly in a 15ml Centrifuge Tube
- Programmable, Automatic Sample Bottle Rinse
DIRECT-TO-VIAL CONCENTRATION
The SuperVap PFC 24 standalone direct-to-vial evaporation/concentration system is the ideal solution for performing the final evaporation and concentration step. SuperVap PFC evaporates the extracts and delivers final extracts in 15ml Centrifuge tubes ready for LC/MS analysis.
HIGH SPEED
- The fastest automated sample processing available
- Vacuum for fast loading of large volume samples as well as samples with heavy particulate
- Modular and Scalable – Run 1 to 6 samples simultaneously, up to 30 samples total
VERSATILE
- Handles a wide range of sample sizes as well as clean and dirty matrix type
- Runs dirty Samples with heavy particulat
- Sample Sizes 2 mL to Unlimite
- Expandable from 1 to 6 modules to fit any budge
- Run a variety of cartridges with different sorbents and all cartridge sizes
- Wash with different solvents or solvent mixes
- Runs up to 5 different methods/sample matrices sequentially
EFFICIENT
- Uses all SPE cartridge sizes
- Positive pressure pumping for loading small volume samples
- Vacuum for large volume, high speed sample loading
- Nitrogen or Vacuum Cartridge drying
Specifications
TurboTrace Sequential Parallel SPE
Dimensions: 15” W x 18” D x 35” H
Weight: 130 lbs.
Gas Requirements: Nitrogen – 20 PSI minimum
Vacuum Requirements: 25” Hg minimum
Pump: Piston Displacement
Flow rate: 0.2 to 15 mL/minute
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: PC based
SuperVapVap Concentration System
Dimensions:7” W x 13” D x 12” H
Weight: 20 lbs.
Gas Requirements: Nitrogen – 20 PSI minimum
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: PC based
Bath: Dry
Consumables
| Part number | Description |
| SPE-ADP-1 | SPE 1ml Cartridge Adapter |
| SPE-ADP-20 | SPE 20ml Cartridge Adapter |
| SPE-ADP-3 | SPE 3ml Cartridge Adapter |
| SPE-ADP-6 | SPE 6ml Cartridge Adapter |
| SPE-BT.5L | SPE Sample Bottle 500ml |
| SPE-BT1 | SPE Sample Bottle 1L |
| SPE-BT1.25L | SPE Sample Bottle 1250ml |
| SPE-BTRC | SPE Sample Bottle Rinse Cap |
| SPE-CAP-1L | SPE Bottle Cap with Loading and Sample Rinse Tubings and Adapters, 1L |
| SPE-CAP-2L | SPE Bottle Cap with Loading and Sample Rinse Tubings and Adapters, 2L |
EconoTrace
An overview of Solid Phase Extraction System
The EconoTrace® Parallel Solid Phase Extraction System is an automated One-Step Extraction and Concentration System is designed to streamline your workflow and increase productivity by automating the manual steps in your sample preparation process. The EconoTrace® Parallel Solid Phase Extraction System uses consistent reproducible positive pressure pumping to replace older manual Liquid-Liquid Extraction techniques, automates existing manual SPE methods and outdated semi-automated instruments.
Applications
Drinking Water
Desalting
Juices
Supports EPA Methods
EPA Method 506 Phthalates and Adipate Esters
EPA Method 508.1 Chlorinated Pesticides, Herbicides, and Organohalides
EPA Method 515.2 Chlorinated Acids
EPA Method 521 Nitrosamines
EPA Method 525.2 Semi-volatiles
EPA Method 526 Semi-volatiles
EPA Method 527 Selected Pesticides and Flame Retardants
EPA Method 528 Phenols
EPA Method 529 Explosives
EPA Method 532 Phenylurea Compounds
EPA Method 535 Chloroacetanilide and other Acetamide Herbicides
EPA Method 548.1 Endothall
EPA Method 549.2 Diquat and Paraquat
EPA Method 550.1 PAH’s
EPA Method 552.1 Haloacetic Acids and Dalapon
EPA Method 553 Benzidines and Nitrogen Containing Pesticides
EPA Method 508.1 Chlorinated Pesticides, Herbicides, and Organohalides
EPA Method 515.2 Chlorinated Acids
EPA Method 521 Nitrosamines
EPA Method 525.2 Semi-volatiles
EPA Method 526 Semi-volatiles
EPA Method 527 Selected Pesticides and Flame Retardants
EPA Method 528 Phenols
EPA Method 529 Explosives
EPA Method 532 Phenylurea Compounds
EPA Method 535 Chloroacetanilide and other Acetamide Herbicides
EPA Method 548.1 Endothall
EPA Method 549.2 Diquat and Paraquat
EPA Method 550.1 PAH’s
EPA Method 552.1 Haloacetic Acids and Dalapon
EPA Method 553 Benzidines and Nitrogen Containing Pesticides
Applications
Extraction of Drugs of Abuse in Urine using Solid Phase Extraction by EconoTrace
Automated One Step Solid Phase Extraction and Concentration of PCBs in Drinking Water
Automated Solid Phase Extraction of EPA 525.2, Semi-Volatile Organic Compounds in Drinking Water
Dioxin in Drinking Water by One Step Solid Phase Extraction
EPA 522; Analysis of 1,4-Dioxane In Drinking Water by Solid Phase Extraction (SPE)
EPA Method 529; Explosives in Drinking Water by Solid Phase Extraction (SPE)
EPA Method 548.1, Endothall in Drinking Water
Extraction of Drugs of Abuse in Urine using Solid Phase Extraction
Polycyclic Aromatic Hydrocarbons in Drinking Water by Solid Phase Extraction (SPE)
Polynuclear Aromatic Hydrocarbons In Water By Automated Solid Phase Extraction and HPLC Analysis
Details
The EconoTrace® Parallel SPE System is designed to streamline your laboratory’s workflow and increase productivity by automating the manual steps in your sample preparation process. The EconoTrace Parallel SPE system automates existing manual SPE techniques and replaces older manual Liquid-Liquid Extraction techniques and outdated semi-automated instruments.
The EconoTrace Parallel SPE system combines extraction, drying and concentration into one step, providing a truly automated total sample prep solution for the laboratory. Load samples onto the EconoTrace Parallel SPE system and start the automated extraction process. After loading the sample onto the SPE cartridge at the programmed flow rate, the drying step is accomplished using Nitrogen. This drying step replaces manual techniques. The analytes of interest are then eluted directly to the SuperVap Concentrator where the concentration process automatically brings the extract to final volume in an autosampler vial, ready for final analysis. Automating these processes into one step ensures the highest quality results in the shortest amount of time and eliminates both loss of compounds of interest from human error and the possibility of contamination.
Economical
Low Cost System for Drinking Water and Clean Matrices
It is a Modular System that can Expand from 1 to 4 Modules to meet the laboratories needs
Runs 2 Samples in Parallel per Module
Runs up to 8 Samples in Parallel
Reduces Errors and Costs
One-Step Automated SPE and Concentration eliminates human error, saves labor costs and reduces solvent usage while increasing your sample throughput
Eliminates Glassware
Separates Aqueous from Organic Waste
Fully Automated
Hyphenates the entire sample prep process: extraction, drying and concentration steps into a one process.
Runs up to eight samples simultaneously
Automatic sample bottle rinse
Concentrates samples up to 250ml directly to a GC vial
High Speed
The fastest automated Positive Pressure sample processing available for SPE cartridges and columns of all sizesPositive pressure pumping for fast, simultaneous loading of samples
Positive pressure pumping for fast simultaneous loading of samples
Versatile
Handles a wide range of sample sizes and all matrix types
Sample Sizes 2 mL to 8 L
Expandable from 1 to 4 modules, 2 samples per module
Efficient
Uses all SPE cartridge and column sizes
Positive pressure pumping for loading samples
Nitrogen drying
Compliant
Complies with existing methods that require positive pressure pumping for the precise delivery of sample and solvents
Dispenses up to six solvents using an HPLC pump to deliver precise volumes and flow rates for sample loading, conditioning and elution
Easy Documentation
Programs and stores an unlimited number of methods and runs on an SD Card
Easy method transfer
Easy-to-use touch screen
Specifications
Dimensions:
15”W x 18”D x 28”H
Weight:
65lbs.
Gas Requirements:
Nitrogen – 20 PSI minimum
Pump:
Piston Displacement Flow
Flow rate: 0.2 to 15ml/minute
Electrical Input:
110/220Volts, 50/60HZ
Controller:
Integrated Touch Screen Control
Consumables
| Part number | Description |
| SPE-ADP-1 | SPE 1ml Cartridge Adapter |
| SPE-ADP-20 | SPE 20ml Cartridge Adapter |
| SPE-ADP-3 | SPE 3ml Cartridge Adapter |
| SPE-ADP-6 | SPE 6ml Cartridge Adapter |
| SPE-BT.5L | SPE Sample Bottle 500ml |
| SPE-BT1 | SPE Sample Bottle 1L |
| SPE-BT1.25L | SPE Sample Bottle 1250ml |
| SPE-BTRC | SPE Sample Bottle Rinse Cap |
| SPE-CAP-1L | SPE Bottle Cap with Loading and Sample Rinse Tubings and Adapters, 1L |
| SPE-CAP-2L | SPE Bottle Cap with Loading and Sample Rinse Tubings and Adapters, 2L |
| SPE-CAR1-C18 | SPE Cartridge 1 gram C18 |
| SPE-CAR1-DVB | SPE Cartridge 1 gram DVB |
| SPE-CAR5-C18 | SPE Cartridge 5 gram C18 |
| SPE-CAR6-DVB | SPE Cartridge 6 gram DVB |
EconoTrace® PFC
Overview of the EconoTrace® Parallel Solid Phase Extraction System for PFAS/PFOS Analysis
Streamlined Solid Phase Extraction of PFAS in Water
The EconoTrace® Parallel Solid Phase Extraction System is an automated one-step solution for the solid phase extraction of PFAS/PFOS in drinking water. Capable of processing up to 8 samples simultaneously, this system simplifies workflows and enhances productivity by automating manual steps in sample preparation.
Key Features
- Positive Pressure Pumping: Ensures consistent and reproducible extraction results.
- Automated Processes: Includes cartridge drying and bottle rinsing for optimal efficiency.
- Integrated Workflow: Delivers extracts directly to the SuperVap PFC system for final concentration and evaporation in 15 mL centrifuge tubes.
- EPA Compliance: Fully supports EPA Methods 533 and 537.1, meeting regulatory standards.
Applications
The EconoTrace® SPE System is designed specifically for:
- Drinking Water Analysis
By automating existing manual SPE methods, the EconoTrace® system reduces errors, improves reproducibility, and accelerates the extraction and concentration processes.
Supports EPA Methods:
EPA Method 533
EPA Method 537.1
More Details
The EconoTrace® Parallel SPE System is designed to streamline your laboratory’s workflow and increase productivity by automating the manual steps in your sample preparation process. The EconoTrace Parallel SPE system automates existing manual SPE techniques and replaces older manual Liquid-Liquid Extraction techniques and outdated semi-automated instruments.
The EconoTrace Parallel SPE system combines extraction, drying and concentration into one step, providing a truly automated total sample prep solution for the laboratory. Load samples onto the EconoTrace Parallel SPE system and start the automated extraction process. After loading the sample onto the SPE cartridge at the programmed flow rate, the drying step is accomplished using Nitrogen. This drying step replaces manual techniques. The analytes of interest are then eluted directly to the SuperVap Concentrator where the concentration process automatically brings the extract to final volume in an autosampler vial, ready for final analysis. Automating these processes into one step ensures the highest quality results in the shortest amount of time and eliminates both loss of compounds of interest from human error and the possibility of contamination.
Details
Economical
Low Cost System for Drinking Water and Clean Matrices
It is a Modular System that can Expand from 1 to 4 Modules to meet the laboratories needs
Runs 2 Samples in Parallel per Module
Runs up to 8 Samples in Parallel
Reduces Errors and Costs
One-Step Automated SPE and Concentration eliminates human error, saves labor costs and reduces solvent usage while increasing your sample throughput
Eliminates Glassware
Separates Aqueous from Organic Waste
Fully Automated
Hyphenates the entire sample prep process: extraction, drying and concentration steps into a one process.
Runs up to eight samples simultaneously
Automatic sample bottle rinse
Concentrates samples directly to a 15ml Centrifuge tube
High Speed
The fastest automated Positive Pressure sample processing available for SPE cartridges
Positive pressure pumping for fast simultaneous loading of samples
Versatile
Handles a wide range of sample sizes and all matrix types
Sample Sizes 2 mL to 8 L
Expandable from 1 to 4 modules, 2 samples per module
Efficient
Uses all SPE cartridge sizes
Positive pressure pumping for loading samples
Nitrogen drying
Compliant
Complies with existing methods that require positive pressure pumping for the precise delivery of sample and solvents
Dispenses up to six solvents using an HPLC pump to deliver precise volumes and flow rates for sample loading, conditioning and elution
Easy Documentation
Programs and stores an unlimited number of methods and runs on an SD Card
Easy method transfer
Easy-to-use touch screen
Specifications
Dimensions:
15”W x 18”D x 28”H
Weight:
65lbs.
Gas Requirements:
Nitrogen – 20 PSI minimum
Pump:
Piston Displacement Flow
Flow rate: 0.2 to 15ml/minute
Electrical Input:
110/220Volts, 50/60HZ
Controller:
Integrated Touch Screen Control
Consumables
| Part number | Description |
| SPE-ADP-1 | SPE 1ml Cartridge Adapter |
| SPE-ADP-20 | SPE 20ml Cartridge Adapter |
| SPE-ADP-3 | SPE 3ml Cartridge Adapter |
| SPE-ADP-6 | SPE 6ml Cartridge Adapter |
| SPE-BT.5L | SPE Sample Bottle 500ml |
| SPE-BT1 | SPE Sample Bottle 1L |
| SPE-BT1.25L | SPE Sample Bottle 1250ml |
| SPE-BTRC | SPE Sample Bottle Rinse Cap |
| SPE-CAP-1L | SPE Bottle Cap with Loading and Sample Rinse Tubings and Adapters, 1L |
| SPE-CAP-2L | SPE Bottle Cap with Loading and Sample Rinse Tubings and Adapters, 2L |
| SPE-CAR1-C18 | SPE Cartridge 1 gram C18 |
| SPE-CAR1-DVB | SPE Cartridge 1 gram DVB |
| SPE-CAR5-C18 | SPE Cartridge 5 gram C18 |
| SPE-CAR6-DVB | SPE Cartridge 6 gram DVB |
SuperVap Concentrators
SuperVap 6
Solvent Evaporation/Concentration: Optimized for Modern Laboratories
Super Vap/6
Solvent evaporation and concentration are critical steps in sample preparation, employed across industries including clinical, food, environmental, pharmaceutical, chemical, and biotechnology. The diversity of sample types and solvents used in these processes requires specialized techniques to meet the needs of various applications.
Challenges in Traditional Evaporation/Concentration Processes
Conventional evaporation and concentration methods rely on systems using nitrogen gas, vacuum pumps, cold traps, and heating technologies. However, these traditional methods often face limitations:
- Inconsistent Results: Variability in evaporation conditions can compromise sample integrity.
- Manual Transfer Errors: The final manual step of transferring the concentrated sample to vials is time-consuming and prone to costly errors.
- Inefficiency: Conventional systems often require significant labor and monitoring.
Benefits of Advanced Dry Evaporation Technologies
Modern dry evaporators, such as the SuperVap® Concentrator, address these challenges by incorporating innovative technologies for efficient, reliable, and precise solvent evaporation.
Key Features of the SuperVap® Concentrator:
- 6-Position Capacity: The system can handle up to six samples simultaneously, with each position accommodating up to 250 mL. This high-capacity design boosts throughput for high-volume laboratories.
- Two Evaporation Modes: Offers two modes of operation—time-based evaporation and automatic endpoint detection—to suit diverse sample preparation needs.
- Automatic Endpoint Detection: Detects when the sample has reached its desired concentration and automatically stops the nitrogen flow and heating, preventing over-concentration and ensuring consistent results.
- Direct-to-Vial Endpoint Delivery: Automatically delivers the concentrated sample directly into autosampler vials, eliminating manual transfer steps. This reduces labor and minimizes cross-contamination or sample loss.
- High-Speed Evaporation: Accelerates the evaporation process with advanced heating technologies, saving valuable time in the laboratory.
- Reproducible Results: Maintains consistent evaporation conditions, ensuring high reproducibility and improved sample integrity.
- Versatility: Supports a wide range of solvents and sample matrices, making it ideal for diverse applications.
- Cost Efficiency: Minimizes solvent usage and reduces labor costs, offering a significant return on investment.
- Ease of Use: Features an intuitive design and programmable operations, allowing for hands-free, unattended evaporation.
Applications of Advanced Evaporation Systems
Dry evaporation technologies are particularly beneficial for laboratories handling:
- Clinical Samples: Achieving precise concentrations for diagnostic analysis.
- Food and Beverage Testing: Concentrating samples for residue and contaminant analysis.
- Environmental Studies: Evaporating solvents from complex matrices like soil and water.
- Pharmaceuticals: Preparing active ingredients for potency testing.
Why Choose Dry Evaporators for Your Laboratory?
Dry evaporation systems, like the SuperVap® Concentrator, provide laboratories with a competitive edge by optimizing workflows, reducing errors, and delivering consistent results. With its 6-position configuration (250 mL capacity per position), two evaporation modes, and automatic endpoint detection, the SuperVap® ensures samples are processed efficiently and accurately.
The automatic endpoint detection feature stops nitrogen flow and heating when the desired endpoint is reached, preventing over-concentration, conserving resources, and preserving sample integrity. Its dual-mode capability—time-based or endpoint detection—offers flexibility for various sample types and workflows.
By adopting advanced evaporation technologies, laboratories can overcome traditional challenges, reduce turnaround times, and achieve superior analytical results.
Product Video
Details
Automated Direct-to-Vial Concentration and Evaporation
The SuperVap system is an automated, standalone, direct-to-vial concentrator that replaces older techniques such as KD, nitrogen blow down and water baths. By automating what were once manual evaporation and concentration processes, the SuperVap concentration system accelerates your sample throughput, lowers labor costs, and improves the consistency of your results by eliminating the variability inherent in manual sample prep procedures.
The SuperVap concentrator sets new a standard for consistency, speed, and reliability of results for an automated sample evaporation and concentration system. It is ideal for the analysis of pesticides, herbicides, Persistent Organic Pollutants (POPs), PCBs, PAHs, pharmaceutical byproducts, and personal care byproducts as well as many other applications. The programmable SuperVap concentrator is a dry, waterless concentrator that can preheat as well as ramp up to final temperature. It automatically senses when the extract is being delivered to each vessel, starts the blow down and then shuts off the nitrogen when final volume is achieved. The concentrated samples are then automatically transferred directly to a vial, eliminating the errors that occur during manual transfer.
Easy-to-Use
The SuperVap concentration system uses a touch screen display for programming, storing, and running methods. Real-time plotting of temperature readings are displayed throughout the process. Simply touch a point on the plot and instantly see the temperature of that point.
Reduces Errors
The SuperVap system performs the entire evaporation and concentration process, automatically, delivering consistent, reproducibly high recoveries for all analytes. Unattended operation of the sample prep process saves time, reduces labor costs, glassware and solvents.
High Recovery of All Analytes
The SuperVap system provides direct-to-vial concentration with automatic endpoint detection and Nitrogen shut off for each vessel
Uses No Water
Uses a robust waterless, dry bath with no electronics submerged in water. It easily and inexpensively captures solvents.
Concentrates up to 6 Samples
Sample Sizes up to 220 mL.
Compact Size
Minimizes Contamination
An integrated HEPA/Carbon filter eliminates outside contamination.
Inexpensive Glassware
Economically priced vessels in 500 µL, 1 mL and direct-to-vial.
Fully Automated
Automatic endpoint detection, nitrogen shutoff, and alarm for each vessel. Programmable heat ramp and nitrogen settings for precise control of the concentration and evaporation process.
Documentation
Every method and run is documented and stored on the SuperVap system for easy retrieval for electronic documentation. A temperature log for each run is also saved and may be downloaded to a PC via a USB port.
Stand Alone or Integrated
The SuperVap concentrator can be easily integrated into existing FMS sample preparation systems. Integration allows for PC-based control and automatic solvent exchange.
Specifications
Dimensions: 13” W x 13” D x 12” H
Weight: 20 lbs.
Gas Requirements: Nitrogen – 20 PSI minimum
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: Touch Screen
Bath: Dry
Consumables
| SVAP-TUB-200M-1000 | 250ml Concentrator tubes 1 ml tip |
| SVAP-TUB-200M-500 | 250ml Concentrator Tube Standard 500 uL Tip |
| SVAP-TUB-200M-GC | 250ml Concentrator Tube Standard GC Vial TIP |
| SVAP-UNI-TEF | Disposable GC Vial Union |
| SVAP-VIAL-GC | GC Vial |
| HPCR-FIL-200 | Hepa/Carbon Filter set-complete |
| SVAP-N2-BLK6 | Evaporator Nitrogen Block, 6 position |
| FMS-TR-2006 | 6 Position Concentrator Tube Rack for 250 ml Tube |
SuperVap 12
Solvent Evaporation/Concentration: Optimized for Modern Laboratories
SuperVap/12
Solvent evaporation and concentration are critical steps in sample preparation, employed across industries including clinical, food, environmental, pharmaceutical, chemical, and biotechnology. The diversity of sample types and solvents used in these processes requires specialized techniques to meet the needs of various applications.
Challenges in Traditional Evaporation/Concentration Processes
Conventional evaporation and concentration methods rely on systems using nitrogen gas, vacuum pumps, cold traps, and heating technologies. However, these traditional methods often face limitations:
- Inconsistent Results: Variability in evaporation conditions can compromise sample integrity.
- Manual Transfer Errors: The final manual step of transferring the concentrated sample to vials is time-consuming and prone to costly errors.
- Inefficiency: Conventional systems often require significant labor and monitoring.
Benefits of Advanced Dry Evaporation Technologies
Modern dry evaporators, such as the SuperVap® 12-Position Evaporator, address these challenges by incorporating innovative technologies for efficient, reliable, and precise solvent evaporation.
Key Features of the SuperVap® 12-Position Evaporator:
- 12-Position Capacity: Processes up to 12 samples simultaneously, accommodating tube sizes ranging from 10 to 40 mL. This design increases throughput for high-demand laboratories.
- Two Evaporation Modes: Offers two modes of operation—time-based evaporation and automatic endpoint detection—to suit diverse sample preparation needs.
- Automatic Endpoint Detection: Detects when the sample has reached its desired concentration and automatically stops the nitrogen flow and heating, preventing over-concentration and ensuring consistent results.
- Direct-to-Vial Endpoint Delivery: Automatically delivers the concentrated sample directly into autosampler vials, eliminating manual transfer steps. This reduces labor and minimizes cross-contamination or sample loss.
- High-Speed Evaporation: Accelerates the evaporation process with advanced heating technologies, saving valuable time in the laboratory.
- Reproducible Results: Maintains consistent evaporation conditions, ensuring high reproducibility and improved sample integrity.
- Versatility: Supports a wide range of solvents and sample matrices, making it ideal for diverse applications.
- Cost Efficiency: Minimizes solvent usage and reduces labor costs, offering a significant return on investment.
- Ease of Use: Features an intuitive design and programmable operations, allowing for hands-free, unattended evaporation.
Applications of Advanced Evaporation Systems
Dry evaporation technologies are particularly beneficial for laboratories handling:
- Clinical Samples: Achieving precise concentrations for diagnostic analysis.
- Food and Beverage Testing: Concentrating samples for residue and contaminant analysis.
- Environmental Studies: Evaporating solvents from complex matrices like soil and water.
- Pharmaceuticals: Preparing active ingredients for potency testing.
Why Choose Dry Evaporators for Your Laboratory?
Dry evaporation systems, like the SuperVap® 12-Position Evaporator, provide laboratories with a competitive edge by optimizing workflows, reducing errors, and delivering consistent results. With its 12-position configuration (accommodating tube sizes from 10 to 40 mL), two evaporation modes, and automatic endpoint detection, the SuperVap® ensures samples are processed efficiently and accurately.
The automatic endpoint detection feature stops nitrogen flow and heating when the desired endpoint is reached, preventing over-concentration, conserving resources, and preserving sample integrity. Its dual-mode capability—time-based or endpoint detection—offers flexibility for various sample types and workflows.
By adopting advanced evaporation technologies, laboratories can overcome traditional challenges, reduce turnaround times, and achieve superior analytical results.
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Product Video
Details
Automated Direct-to-Vial Concentration and Evaporation
The SuperVap system is an automated, standalone, direct-to-vial concentrator that replaces older techniques such as KD, nitrogen blow down and water baths. By automating what were once manual evaporation and concentration processes, the SuperVap concentration system accelerates your sample throughput, lowers labor costs, and improves the consistency of your results by eliminating the variability inherent in manual sample prep procedures.
Specifications
Dimensions: 13” W x 13” D x 12” H
Weight: 20 lbs.
Gas Requirements: Nitrogen – 20 PSI minimum
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: Touch Screen
Bath: Dry
Consumables
| SVAP-TUB-060M-1000 | 50 ml Concentrator tubes 1 ml tip |
| SVAP-TUB-060M-500 | 50ml Concentrator Tube Standard 500 uL Tip |
| SVAP-TUB-060M-GC | 50ml Concentrator Tube Standard GC Vial TIP |
| SVAP-VIA-020M-000 | 20 ml Concentrator vial. pack of 500 |
| SVAP-VIA-040M-000 | 40 ml Concentrator vial. pack of 500 |
| SVAP-VIA-060M-000 | 60ml Concentrator vial, pack of 500 |
| SVAP-BLK-12-020 | SuperVap Concentrator block – 12 Position for 20 ml Concentration vials |
| SVAP-BLK-12-040 | SuperVap Concentrator block – 12 Position for 40 ml Concentration vials |
| SVAP-BLK-12-060 | SuperVap Concentrator block – 12 Position for 60 ml Concentration vials |
SuperVap 24
Solvent Evaporation/Concentration
SuperVap 24
Solvent evaporation and concentration are essential steps in sample preparation, widely used in industries such as clinical, food, environmental, pharmaceutical, chemical, and biotechnology. Given the diversity of sample types and solvents, no single method fits all applications. Advanced evaporation systems have been developed to address specific requirements, leveraging technologies like nitrogen gas, vacuum pumps, cold traps, and heating systems to deliver precision and efficiency.
Overcoming Challenges in Solvent Evaporation
Traditional evaporation and concentration techniques often face limitations:
- Inconsistent Results: Variability in evaporation conditions can compromise sample integrity.
- Labor-Intensive Processes: Manual transfer steps increase the risk of errors and contamination.
- Time Constraints: Conventional methods require extended monitoring and hands-on labor.
Modern evaporation technologies, including 24-position systems, provide scalable solutions that streamline workflows, reduce errors, and improve overall efficiency.
Key Features of the 24-Position Evaporator
- High-Capacity Processing: Handles up to 24 samples simultaneously, significantly increasing throughput for high-demand laboratories.
- Tube Compatibility: Accommodates a wide range of tube sizes, supporting volumes from 1o microliter to 1 milliliter mL, making it suitable for Micro evaporation..
- Rapid Evaporation: Advanced heating technologies ensure faster evaporation times, reducing turnaround and increasing productivity.
- Reproducible Results: Consistent conditions and precise automation ensure reproducible outcomes for all samples.
- Ease of Use: Features an intuitive interface with programmable operations for hands-free, unattended evaporation.
Applications of the 24-Position Evaporator
Super Vap/24 is ideal for a range of industries and applications, including:
- Clinical Diagnostics: Concentrating samples for diagnostic and research purposes.
- Food and Beverage Testing: Analyzing residues, contaminants, and active ingredients.
- Environmental Studies: Preparing samples from complex matrices like soil and water for analysis.
- Pharmaceuticals: Concentrating active ingredients and excipients for potency testing.
- Biotechnology: Streamlining workflows for biochemical and molecular studies.
Benefits of Using a 24-Position Evaporator
- Maximized Throughput: The 24-sample capacity allows laboratories to process more samples in less time, making it ideal for high-throughput environments.
- Labor Savings: Automated processes reduce the need for manual intervention, freeing up valuable staff time.
- Versatility: Accommodates a variety of sample types and solvents, meeting the needs of multiple industries.
Why Choose a 24-Position Evaporator for Your Laboratory?
The 24-position evaporator sets a new standard in solvent evaporation and concentration, offering unparalleled capacity, precision, and reliability. Its dual operation modes, compatibility with a variety of tube sizes, and advanced automation features make it a game-changer for laboratories aiming to optimize their workflows.
Product Video
Details
Automated Direct-to-Vial Concentration and Evaporation
The SuperVap system is an automated, standalone, direct-to-vial concentrator that replaces older techniques such as KD, nitrogen blow down and water baths. By automating what were once manual evaporation and concentration processes, the SuperVap concentration system accelerates your sample throughput, lowers labor costs, and improves the consistency of your results by eliminating the variability inherent in manual sample prep procedures.
Specifications
Dimensions: 13” W x 13” D x 12” H
Weight: 20 lbs.
Gas Requirements: Nitrogen – 20 PSI minimum
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: Touch Screen
Bath: Dry
Consumables
| SVAP-VIA-002M-000 | 2 ml Concentrator vial, pack of 100 |
| SVAP-VIA-004M-000 | 4 ml Concentrator vial ,pack of 100 |
| SVAP-BLK-24-002 | SuperVap Concentrator block – 24 Position for 2 ml Concentration vials |
| SVAP-BLK-24-004 | SuperVap Concentrator block – 24 Position for 4 ml Concentration vials |
SuperVap PFC Concentrator Designed for PFAS Analysis
Automated Concentration and Evaporation
The SuperVap system is an automated, standalone, direct-to-vial concentrator that replaces older techniques such as KD, nitrogen blow down and water baths. By automating what were once manual evaporation and concentration processes, the SuperVap concentration system accelerates your sample throughput, lowers labor costs, and improves the consistency of your results by eliminating the variability inherent in manual sample prep procedures.
The SuperVap concentrator sets new a standard for consistency, speed, and reliability of results for an automated sample evaporation and concentration system. It is ideal for the analysis of PFAS/PFOS, pharmaceutical byproducts, and personal care byproducts as well as many other applications. The programmable SuperVap concentrator is a dry, waterless concentrator that can preheat as well as ramp up to final temperature. It automatically shuts off the heat and nitrogen at a designated time. The operator can then return to finish the final steps of the evaporation process to achieve final volume or dryness.
Easy-to-Use
The SuperVap concentration system uses a touch screen display for programming, storing, and running methods. Real-time plotting of temperature readings are displayed throughout the process. Simply touch a point on the plot and instantly see the temperature of that point.
Reduces Errors
The SuperVap system performs the entire evaporation and concentration process, automatically, delivering consistent, reproducibly high recoveries for all analytes. Unattended operation of the sample prep process saves time, reduces labor costs, glassware and solvents.
High Recovery of All Analytes
The SuperVap system provides direct-to-vial concentration with automatic timed endpoint and Nitrogen shut off for each vessel
Uses No Water
Uses a robust waterless, dry bath with no electronics submerged in water. It easily and inexpensively captures solvents.
Concentrates up to 24 Samples
Sample Sizes most 15mL conical plastic vessels
Compact Size
Minimizes Contamination
An integrated HEPA/Carbon filter eliminates outside contamination.
Fully Automated
Automatic timed endpoint, nitrogen shutoff, and alarm. Programmable heat ramp and nitrogen settings for precise control of the concentration and evaporation process.
Documentation
Every method and run is documented and stored on the SuperVap system for easy retrieval for electronic documentation. A temperature log for each run is also saved and may be downloaded to a PC via a USB port.
System Video
Specifications
Dimensions: 13” W x 13” D x 12” H
Weight: 20 lbs.
Gas Requirements: Nitrogen – 20 PSI minimum
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: Touch Screen
Bath: Dry
Consumables
| SVAP-VIA-002M-000 | 2 ml Concentrator vial, pack of 100 |
| SVAP-VIA-004M-000 | 4 ml Concentrator vial ,pack of 100 |
| SVAP-BLK-24-002 | SuperVap Concentrator block – 24 Position for 2 ml Concentration vials |
| SVAP-BLK-24-004 | SuperVap Concentrator block – 24 Position for 4 ml Concentration vials |
Sample Clean-Up Systems
Economic Sample Cleanup for Dioxins and PCBs
Imagine performing the Sample Cleanup process for POPs analysis in Liquids and Solids automatically in as little as 30 minutes.
Built on 25 years of FMS, Inc. experience and technology that has processed millions of samples for the analysis of Dioxin and PCBs
FMS introduces a new family of integrated, economical sample cleanup systems that combine manual sample prep steps into one automated process. EconoPrep® systems perform sample cleanup, fractionation and concentration for up to eight samples simultaneously in less than 1 hour, while delivering the highest recoveries and best results for all target Dioxin and PCB analytes. The systems are programmed and controlled via an easy-to-use touch screen and methods are stored on SD cards. A flexible system that allows running a single sample preparation step, such as sample cleanup, fractionation or concentration is also an option.
Affordable Automation of Sample Cleanup for the analysis of Dioxins and PCBs for Laboratories of any size.
FMS, Inc. Introduces the New Chemistry Kit Rental Program for the Industry Standard EconoPrep® Multicolumn Cleanup System for Dioxins and PCBs:
- Allows the laboratory to acquire equipment without the outlay of capital funds
- A program designed to fit within a laboratory’s budgetary constraints better than a capital purchase
- Offers a program that could fit within a laboratory’s purchasing departments constraints
- It will allow laboratories to implement automation quickly and not have to wait for months or years
Applications
Automated Sample Preparation for Dioxins and Furans in Stack Emissions
Polychlorinated Dibenzo-p-dioxins, Furans and Biphenyls in Fish Automated Sample Processing
Automated Extraction and Cleanup of Egg Yolk Dioxins and Furans
Automated Extraction and Clean Up of Crab Meat Dioxins and Furans
Dioxins, Furans, and PCBs in Peanut Butter Samples Processed with Automated Extraction and Clean Up
One Step Extraction, Cleanup and Concentration for PBDEs in Soil
Automated Extraction and Clean Up of Wood Boiler Ash Samples Dioxins, Furans, and PCBs
Details
Simultaneously perform eight Sample Cleanups and Concentrations in less than 1 hour
The EconoPrep systems are integrated, economical sample preparation systems that combine the sample cleanup, and evaporation steps into one automated process.
Unattended Sample Preparation
Install the cleanup columns on the system, push the “Run” button and walk away. The EconoPrep systems will automatically load a sample and perform the entire sample preparation process unattended, in virtually one step. The final fraction is ready for analysis by GC, LC, or GC/LC/MS.
Same Day Turn Around for Multiple Samples
Because the EconoPrep can process eight samples in parallel sample cleanup, and concentration. EconoPrep systems are able to turn around up to 64 samples in a day.
Greener Approach Dramatically Reducing Solvent Consumption
The greater efficiency with which the EconoPrep systems perform cleanup reduces solvent consumption.
-Solvent Consumption as low as 120ml
Dramatic Savings in Time and Resources
EconoPrep systems perform the complete preparation of eight samples in just a 30 minutes, instead of days. This results in time and labor savings as well as high throughput.
Low Background Automated Sample Prep
The advanced, closed loop system design combined with pre-packed, disposable columns deliver cleaner backgrounds and eliminate cross contamination.
Wide range of pre-packed, disposable cleanup columns
A wide variety of economical, pre-packed, disposable cleanup columns are available for use with EconoPrep systems. These columns are configured in a variety of sizes and packing material types ? from standard multi-layered ABN silica to custom made columns.
Disposable Columns used for Dioxins and
PCBs, analysis:
1. Multi-layered ABN silica
2. Alumina
3. Carbon
4. High capacity acid silica (optional used for fatty samples, these column remove 5 to 7 grams of fat
Robust and Maintainable
The modular, flexible design of EconoPrep systems virtually eliminates downtime and makes them the most easily to maintain systems in today’s laboratories. Each system channel operates independently of the other channels, so if one channel malfunctions the others still work. Should a module malfunction, laboratory personnel can replace it on-site and the exposed construction makes parts accessible for easy replacement.
Specifications
Weights:
Control module = 22lbs
EconoPrep valve module = 31lbs
Control Module Base = 6 lbs
Single Base = 3 lbs
EconoPrep2 = 62lbs
EconoPrep4 = 97lbs
EconoPrep6 = 132lbs
EconoPrep8 = 167lbs
Small cart = 35lbs
Small tray = 20lbs
Medium cart = 40lbs
Medium tray = 25lbs
Large cart = 45lbs
Large tray = 35lbs
Dimensions:
EconoPrep2 = 16”(41cm)W X 26”(65cm) H X 17”(43cm) D
EconoPrep4 = 25”(63cm)W X 26”(65cm) H X 17”(43cm) D
EconoPrep6 = 34”(86cm)W X 26”(65cm) H X 17”(43cm) D
EconoPrep2 = 43”(110cm)W X 26”(65cm) H X 17”(43cm) D
Pump:
Piston Displacement Flow
Flow rate: 0.2 to 15ml/minute
Electrical Input:
110/220Volts, 50/60HZ
Controller:
Integrated Touch Screen Control
Consumables
EconoPrep Column Kits:
| Dioxin & PCB Kits | ||
| Part Number | Includes | Description |
| EHCEP-KT5.0 | Extra High Capacity Plus DIOXIN/PCB Kit 5g Fat Removal Capacity | |
| SNEH-ACD-050 | Extra High Capacity Acid Silica Column | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNAL-BAS-011 | 11G Basic Alumina Column | |
| SNCA-C45-034 | Carbon/Celite Column | |
| HCCEP-KT2.5 | High Capacity DIOXIN/PCB Kit 2.5 Fat Removal Capacity | |
| SNHC-ACD-029 | High Capacity Acid Silica Columns | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNAL-BAS-011 | 11G Basic Alumina Column | |
| SNCA-C45-034 | Carbon/Celite Column | |
| MIDEP-KT1.0 | Classical Plus DIOXIN/PCB Kit 1g Fat Removal Capacity | |
| SNMI-ACD-009 | Medium Capacity Acid Silica Column | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNAL-BAS-011 | 11G Basic Alumina Column | |
| SNCA-C70-034 | Carbon/Celite Column | |
| CLSEP-KT0.5 | Classical DIOXIN/PCB Kit .5g Fat Removal Capacity | |
| SNCL-ACD-006 | Classical Acid Silica Column | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNAL-BAS-011 | 11G Basic Alumina Column | |
| SNCA-C70-034 | Carbon/Celite Column |
EconoPrep/110 (EP-110) - Automated Dioxins and PCBs Sample Prep
| Green Technology | Zero DCM |
| Fast | 30 to 45 minutes |
| High Throughput | Up to 8 Samples in Parallel |
| Low Solvent | As Low As 110ml per Sample |
| Fully Automated | From Sample Loading to GC Vial |
| Expandable | From 2 to 8 samples |
| Quality Consumables | Guaranteed Certified Columns |
| Economical | Column Kits to meet your Sample Matrix |
| Reliable | Easy to Maintain |
Imagine performing the Sample Cleanup process for POPs analysis in liquids and solids automatically in as little as 30 minutes.
Built on 25 years of FMS, Inc. experience and technology that has processed millions of Dioxin samples, FMS introduces a new family of integrated, economical sample cleanup systems that combine manual sample prep steps into one automated process. The EP-110 systems perform sample cleanup, fractionation and concentration for up to eight samples simultaneously in less than 1.5 hours, while delivering the highest recoveries and best results for all target Dioxin and PCB analytes. The systems are programmed and controlled via an easy-to-use touch screen and methods are stored on SD cards. A flexible system that automates sample preparation steps, such as sample loading, wash, elution and fraction collection, all in one step. An integrated concentrator concentrates the final extract automatically and delivers the final extract in a GC vial ready for GC/MS analysis.
Product Video
Applications
From Samples to Report: Rapid Dioxin/PCB Analysis Using Fully Automated Extraction, Sample Cleanup, and Concentration, Analyzed and Reported by the Agilent® 7010B GC/TQ
POPs Extraction and Cleanup using Low Solvent Green Total EconoPrep
Low Solvent Extraction and Zero DCM Sample Cleanup for POPs Analysis
Details
Green Technology: Zero DCM
Fast: 30 to 45 minutes
Fat / Lipid Removal: Capacity up to 7 Grams
High Throughput: Up to 8 Samples in Parallel
Low Solvent: As Low As 90 ml per Sample or as High 180ml based on Lipid content
Fully Automated: From Sample Loading to GC Vial
Expandable: From 2 to 8 samples
Quality Consumables: Guaranteed Certified Columns
Economical: Column Kits to meet your Sample Matrix Fat/Lipid content
Reliable: Easy to Maintain
New! Easy To Use: Quick connect snap columns
Green Technology: Zero DCM
The EP-110 uses Zero DCM in the cleanup process. By design it produces greater efficiency to perform clean up and it greatly reduces solvent consumption.
Fast: 30 to 45 minutes
Depending on the Sample Matrix and Lipid content samples can be run in 30 to 45 minutes. Column kits designed to meet different sample lipid content allow for fast sample processing. The system can turn around up to 64 samples in a day.
Low Solvent: As Low As 110ml per Sample
Column Kits designed for samples with different lipid content allow for using the lowest possible amount of solvent to process a sample.
Expandable: From 2 to 8 samples
The EP-110 is modular and can be expanded to fit the needs of any lab. Each module can handle 2 samples in parallel. The system can have up to 4 modules running 8 samples in parallel.
Quality Consumables: Guaranteed
Certified Columns
FMS’s Column Consumables are Certified and Guaranteed for cleanliness, high recoveries and performance.
Fat / Lipid Removal: Capacity 0.15 to
7 Grams
A wide variety of economical “cleanup column kits” are available for Dioxin and PCB sample preparation.
New: Easy to Use Quick Connect Snap Columns
To streamline the ease and use of columns, FMSintroduces the Quick Connect Snap Columns
sample cleanup, and evaporation steps into one automated process. The EP-110 processes eight samples in parallel including sample cleanup, and concentration. The systems are able to be turned around up to 64 samples in a day.
Automated Sample Loading
Install the cleanup columns on the system, push the “Run” button and walk away. The EP-110 will automatically load the sample and perform the entire sample preparation process unattended, in virtually one step. The final fractions are ready for analysis by GC/MS.
Reliable: Easy to Maintain
The modular, flexible design of EconoPrep systems virtually eliminates downtime and
makes them the most easily to maintain systems in today’s laboratories. Each system module operates independently of the other modules,
so if one module malfunctions the others still work. Should a module malfunctions, laboratory personnel can easily replace it on-site.
Applications examples
Liquids:
Egg Yolk
Milk
Food Oils
Serum
Water
Waste Water
Solids:
Fish
Feed
Meat
Soils
Sludge
Fly Ash
Specifications
Weights:
Control module = 22lbs
EP110 valve module = 31lbs
Control Module Base = 6 lbs
Single Base = 3 lbs
EP110 2 = 62lbs
EP110 4 = 97lbs
EP110 6 = 132lbs
EP110 8 = 167lbs
Small cart = 35lbs
Small tray = 20lbs
Medium cart = 40lbs
Medium tray = 25lbs
Large cart = 45lbs
Large tray = 35lbs
Dimensions:
EP110 2 = 16”(41cm)W X 26”(65cm) H X 17”(43cm) D
EP110 4 = 25”(63cm)W X 26”(65cm) H X 17”(43cm) D
EP110 6 = 34”(86cm)W X 26”(65cm) H X 17”(43cm) D
EP 110 8 = 43”(110cm)W X 26”(65cm) H X 17”(43cm) D
Pump:
Piston Displacement Flow
Flow rate: 0.2 to 15ml/minute
Electrical Input:
110/220Volts, 50/60HZ
Controller:
Integrated Touch Screen Control
Consumables
Dioxin & PCB Kits
| Part Number | Includes | Description |
| EHCLS-KT05.0DP | Extra High Capacity DIOXIN/PCB Kit 5g Fat Removal Capacity | |
| SNEH-ACD-050 | Extra High Capacity Acid Silica Column | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNAL-BAS-006 | 6G Basic Alumina Column | |
| SNCA-C45-034 | Carbon/Celite Column | |
| HCCLS-KT2.5DP | High Capacity DIOXIN/PCB Kit 2.5 Fat Removal Capacity | |
| SNHC-ACD-029 | High Capacity Acid Silica Columns | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNAL-BAS-006 | 6G Basic Alumina Column | |
| SNCA-C45-034 | Carbon/Celite Column | |
| MIDLS-KT1.0DP | Classical Plus DIOXIN/PCB Kit 1g Fat Removal Capacity | |
| SNMI-ACD-009 | Medium Capacity Acid Silica Column | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNCL-BAS-004 | 4G Basic Alumina Column | |
| SNCA-C70-034 | Carbon/Celite Column | |
| CLSLS-KT0.DP | Classical DIOXIN/PCB Kit .5g Fat Removal Capacity | |
| SNCL-ACD-006 | Classical Acid Silica Column | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNCL-BAS-004 | 4G Basic Alumina Column | |
| SNCA-C70-034 | Carbon/Celite Column |
Dioxin Kits
| Part Number | Includes | Description |
| EHCLS-KT05.0DI | Extra High Capacity DIOXIN Kit 5g Fat Removal Capacity | |
| SNEH-ACD-050 | Extra High Capacity Acid Silica Column | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNCA-C45-034 | Carbon/Celite Column | |
| HCCLS-KT2.5DI | High Capacity DIOXIN Kit 2.5 Fat Removal Capacity | |
| SNHC-ACD-029 | High Capacity Acid Silica Columns | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNCA-C45-034 | Carbon/Celite Column | |
| MIDLS-KT1.0DI | Classical Plus DIOXIN Kit 1g Fat Removal Capacity | |
| SNMI-ACD-009 | Medium Capacity Acid Silica Column | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNCA-C70-034 | Carbon/Celite Column | |
| CLSLS-KT0.5DI | Classical DIOXIN Kit .5g Fat Removal Capacity | |
| SNCL-ACD-006 | Classical Acid Silica Column | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNCA-C70-034 | Carbon/Celite Column | |
Power Prep/NG - Dioxins and PCBs Sample Prep System
An Overview of Multi-Column Sample Cleanup
Sample cleanup is a very important step because methods often don’t respond to the analyte in its in-situ form, or the results can be distorted by interfering species. Column cleanup is used to eliminate interferences that can occur in the sample matrices. Multi-column cleanup procedures use multiple column chemistries to remove interferences and fractionate analytes of interest from complicated sample matrices.
PowerPrep Multi-Column Sample Cleanup System
The PowerPrep™ Multi-Column Sample Cleanup System is the only automated sample processing system of its kind available today. It is an automated liquid chromatography system that performs simultaneous sample processing unattended. The total sample preparation process – sample loading, washing, elution, fraction collection and concentration — is performed automatically. The PowerPrep Multi-Column Sample Cleanup System is designed specifically to replace the difficult, error prone, labor intensive manual processes involved in sample cleanup for trace analysis. For the trace analysis of Persistent Organic Pollutants in all sample matrices, the PowerPrep Multi-Column Sample Cleanup System performs sample cleanup in a matter of hours, not days. Its modular design allows easy maintenance and expansion. The Sample Processing Module is designed for Multi-column sample cleanup and fractionation and the patented pump ensures precise solvent delivery to achieve reproducible results. The Multi-Column Sample Processing Module can be easily swapped out to perform single column sample cleanup chemistries which allows your lab to use the PowerPrep System for automating other sample prep processes. Samples are cleaned up and directly fractionated to the SuperVap Concentrator for unattended transfer and concentration directly to a vial.
The SuperVap Concentrator is a dry, waterless, programmable system that can preheat as well as ramp up to final temperature. When the concentrator senses that the extracts are being delivered to each vessel it automatically starts the nitrogen blow down. It then shuts off the nitrogen blow down when each extract has achieved final volume.
Applications
EPA 1613 PCDD-Fs and PCBs Analysis in Pet Food Using Automated Extraction and Cleanup
EPA 1613 Dioxins and Furans in Freeze-Dried and Regular Milk by PLE and PowerPrep
EPA 1613 Dioxins and Furans in Egg Yolk by PLE
EPA 1613 Dioxins and Furans in Crab Meat by PowerPrep and PLE
EPA 1613 and 1668C POPs Extraction and CleanUp using Low Solvent Green Total EconoPrep
EPA 1613 and 1668 PCDDs PCDFs and PCBs in Fish by Automated Sample Processing
EPA 1613 and 1668 Dioxins PCBs and PBDEs in Human Serum by PLE and PowerPrep
EPA 1613 and 1668 Dioxins Furans and PCBs in Peanut Butter Samples by PLE and PowerPrep
EPA 1613 and 1668 Dioxins Difurans and PCBs in Food Oil by PowerPrep
Cooking up a Solution – Same Day Testing of Dioxins and PCBs for Food Safety is Now Feasible
The Analysis of Chlorinated Dioxins, Difurans and Polychlorinated Biphenyls in Edible Oils
The Analysis of Chlorinated Dioxins, Difurans and Polychlorinated Biphenyls in Edible Oils
The Analysis of Chlorinated Dioxins, Difurans in Pet Food
Automated Extraction and Cleanup of Egg Yolk Dioxins and Furans
Automated Extraction and Clean Up of Crab Meat Dioxins and Furans
Dioxins, Furans, and PCBs in Peanut Butter Samples Processed with Automated Extraction and Clean Up
Polychlorinated Dibenzo-p-dioxins, Furans and Biphenyls in Fish Automated Sample Processing
Details
Automated Sample Cleanup for Trace Analysis
The Powerprep Multi-Column Sample Cleanup system automates error prone, tedious, manual sample cleanup and fractionation steps in the laboratory. It replaces older manual techniques by automating the sample loading, washing, elution, fractionation and evaporation steps of the process. It increases laboratory throughput by performing sample cleanup and fractionation in hours instead of days.
The Powerprep Multi-Column Sample Cleanup system automates error prone, tedious, manual sample cleanup and fractionation steps in the laboratory. It replaces older manual techniques by automating the sample loading, washing, elution, fractionation and evaporation steps of the process. It increases laboratory throughput by performing sample cleanup and fractionation in hours instead of days.
Rapid Sample Processing
The Power-Prep system, that automates the entire manual sample cleanup process, processes samples in hours versus days.
Cost Effective and Reliable Analysis
The system performs the entire column chromatography, automatically and unattended, and delivers consistent, reproducible recoveries for all analytes. Unattended operation of the system saves labor and time, reducing glassware and solvents. It automates difficult manual sample cleanup procedures specifically for the trace analysis of Dioxins, BFRs, PCBs, Pesticides and PAHs.
High Recovery of all Analytes
FMS columns are certified and guaranteed for the cleanup of samples for the trace analysis of Dioxins, PAHs, PBDEs, and PCBs producing the highest recoveries for all analytes of interest.
Modular, Expandable, and Affordable
The PowerPrep system is modular and can be expanded from 1 to 6 samples. Both expansion and module replacement are done via FMS’s quick connect modules reducing system down time, increasing laboratory throughput and eliminating cross contamination from sample to sample.
Disposable Columns
The PowerPrep System uses proprietary FMS columns made from teflon and contain packings such as multi-silica, acidic silica, basic silica, neutral silica, alumina, carbon and florisil. FMS columns are tested for purity and performance. Prior to shipment they are certified and guaranteed.
Easy Documentation
Programs and stores an unlimited number of methods and runs.
Specifications
Dimensions: 15” W x 18” D x 35” H
Weight: 130 lbs.
Pump: Piston Displacement
Flow rate: 0.2 to 15 mL/minute
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: PC based
SuperVap Concentration System
Dimensions:13” W x 13” D x 12” H
Weight:20 lbs.
Gas Requirements: Nitrogen – 20 PSI minimum
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: PC based
Bath: Dry
Consumables
| Consumables: | Dioxin & PCB Kits: | ||||
| Part Number: | Description: | Part Number: | Description: | ||
| Low capacity Columns | EHCNG-KT05.0DP | Extra High Capacity DIOXIN/PCB Kit 5g Fat Removal Capacity | |||
| LCDS-ABN-STD | Low Capacity Disposable Silica ABN Column | SNEH-ACD-050 | Extra High Capacity Acid Silica Column | ||
| LCDA-BAS-6 | Low Capacity Disposable Basic Alumina Column | SNLC-BAN-004 | Basic and Neutral Silica Column | ||
| CLDC-CCE-34 | SNAL-BAS-006 | 6G Basic Alumina Column | |||
| Low Capacity PCB Free Columns | SNCA-C34-034 | Carbon/Celite Column | |||
| PCBL-ABN-STD | PCB Free Low Capacity Disposable Silica ABN Column | ||||
| PCBL-BAS-6 | PCB Free Low Capacity Disposable Alumina (6g) Column | HCCNG-KT2.DP | High Capacity DIOXIN/PCB Kit 2.5 Fat Removal Capacity | ||
| PCBC-CCE-34 | PCB Free Classical Disposable Carbon/celite Column .34g | SNHC-ACD-029 | High Capacity Acid Silica Columns | ||
| Low Capacity PBDE free columns | SNLC-BAN-004 | Basic and Neutral Silica Column | |||
| PBDEL-BAS-6 | PBDE Free Low Capacity Disposable Alumina (6g) Column | SNAL-BAS-006 | 6G Basic Alumina Column | ||
| PBDEL-ABN-STD | PBDE Free Low Capacity Disposable Silica ABN Column | SNCA-C34-034 | Carbon/Celite Column | ||
| Classical Columns | |||||
| CLDS-ABN-STD | Classical Disposable Silica ABN Column | MIDNG-KT1.0DP | Classical Plus DIOXIN/PCB Kit 1g Fat Removal Capacity | ||
| CLDA-BAS-11 | Disposable Basic Alumina (11g) Column | SNMI-ACD-009 | Medium Capacity Acid Silica Column | ||
| CLDC-CCE-34 | Disposable Carbon/Celite (.34g) Column | SNLC-BAN-004 | Basic and Neutral Silica Column | ||
| HCDS-ABN-STD | High Capacity Disposable ABN Silica Column | SNCL-BAS-004 | 4G Basic Alumina Column | ||
| HCDS-ACD-STD | High Capacity Disposable Acidic Silica Column | SNCA-C34-034 | Carbon/Celite Column | ||
| HCDS-ABN-STD-TFC | High Capacity Disposable ABN Silica Column with Teflon Chip | ||||
| HCDS-ACD-STD-TFC | High Capacity Disposable Acidic Silica Column with Teflon Chip | CLSNG-KT0.5DP | Classical DIOXIN/PCB Kit .5g Fat Removal Capacity | ||
| PCB Free classical Columns | SNCL-ACD-006 | Classical Acid Silica Column | |||
| PCBS-ABN-STD | PCB Free Classical Disposable Silica ABN Column | SNLC-BAN-004 | Basic and Neutral Silica Column | ||
| PCBA-BAS-11 | PCB Free Disposable Alumina (11g) Column | SNCL-BAS-004 | 4G Basic Alumina Column | ||
| PCBC-CCE-34 | PCB Free Classical Disposable Carbon Column | SNCA-C34-034 | Carbon/Celite Column | ||
| PCB-HCDS-ABN | PCB Free High Capacity Disposable ABN Silica Column | ||||
| PCB-HCDS-ACD | PCB Free High Capacity Disposable Acidic Silica Column | ||||
| PBDE Free classical columns | |||||
| PBDES-ABN-STD | PBDE Free Classical Disposable Silica ABN Column | ||||
| PBDEA-BAS-11 | PBDE Free Disposable Alumina (11g) Column | ||||
| PBDEC-CCE-34 | PBDE Free Classical Disposable Carbon/Celite Column | ||||
| PBDE-HCDS-ABN | PBDE Free High Capacity Disposable ABN Silica Column | ||||
| PBDE-HCDS-ACD | PBDE Free High Capacity Disposable Acidic Silica Column | ||||
| Silver Nitrate /Silica columns | |||||
| CLDS-ABN-SNT | Classical Disposable ABN Silica + Silver Nitrate Column | ||||
| PCBS-ABN-SNT | PCB Free Classical Disposable ABN Silica + Silver Nitrate Column | ||||
| PBDES-ABN-SNT | PBDE Free Classical Disposable ABN Silica + Silver Nitrate Column | Dioxin Kits: | |||
| HCDS-ABN-SNT | High Capacity Disposable ABN Silica + Silver Nitrate Column | ||||
| Carbon/Silica columns | Part Number | Description | |||
| CLDC-CSI-2 | Disposable Carbon/Silica (2g) Column | EHCNG-KT05.0DI | Extra High Capacity DIOXIN Kit 5g Fat Removal Capacity | ||
| PCBC-CSI-2 | PCB Free Disposable Carbon/Silica (2g) Column | SNEH-ACD-050 | Extra High Capacity Acid Silica Column | ||
| PBDEC-CSI-2 | PBDE Free Disposable Carbon/Silica (2g) Column | SNLC-BAN-004 | Basic and Neutral Silica Column | ||
| Florisil columns | SNCA-C34-034 | Carbon/Celite Column | |||
| CLDF-FLR-705 | Classical Disposable Florisil (7.5g) Column | ||||
| PCBF-FLR-705 | PCB Free Disposable Florisil Column | HCCNG-KT2.5DI | High Capacity DIOXIN Kit 2.5 Fat Removal Capacity | ||
| Miscellaneous columns | SNHC-ACD-029 | High Capacity Acid Silica Columns | |||
| CLDF-FLR-705 | Classical Disposable Florisil (7.5g) Column | SNLC-BAN-004 | Basic and Neutral Silica Column | ||
| CLDS-ACD-8 | Classical Disposable Acidic Silica (8g) Column | SNCA-C34-034 | Carbon/Celite Column | ||
| CLDS-NSS-60 | Classical Disposable Neutral Silica (6g) Column | ||||
| PCBA-5BAS-11 | PCB Free Disposable 0.005 Deactivated Alumina (11g) Column | MIDNG-KT1.0DI | Classical Plus DIOXIN Kit 1g Fat Removal Capacity | ||
| PBDEA-5BAS-11 | PBDE Free Disposable 0.005 Deactivated Alumina (11g) Column | SNMI-ACD-009 | Medium Capacity Acid Silica Column | ||
| Hex Fittings | SNLC-BAN-004 | Basic and Neutral Silica Column | |||
| CLTF-FIT-0 | Fitting Teflon Hex For Classical Teflon Columns | SNCA-C34-034 | Carbon/Celite Column | ||
| CLTF-FIT-25 | Fitting Teflon Hex For High Capacity Columns | ||||
| Tefzel fittings | CLSNG-KT0.5DI | Classical DIOXIN Kit .5g Fat Removal Capacity | |||
| UNI-TFZ-28 | Fitting Tefzel Union | SNCL-ACD-006 | Classical Acid Silica Column | ||
| MLU-TFZ-28 | Fitting Tefzel Male Luer | SNLC-BAN-004 | Basic and Neutral Silica Column | ||
| FLU-TFZ-28 | Fitting Tefzel Female Luer | SNCA-C34-034 | Carbon/Celite Column | ||
| Delrin Fittings | |||||
| UNI-DEL-28 | Fitting Delrin Union | ||||
| MLU-DEL-28 | Fitting Delrin Male Luer | ||||
| FLU-DEL-28 | Fitting Delrin Female Luer | ||||
| Fritz | |||||
| FRZ-TFE-678 | Small Fritz | ||||
| FRZ-TFE-901 | Large Fritz | ||||
| Vial & Syringe | |||||
| TUBE-CEN-15 | Glass Sample Vials With Caps 15ml | ||||
| SYRI-POL-10 | Polypropylene Syringes |
EPH Fractionation
The PowerPrep EPH High Throughput Sample Fractionation System
The PowerPrep™ EPH Fractionation system performs fractionation and sample cleanup for up to 30 samples in less than one hour, producing the highest recoveries and best results for aliphatic and aromatic hydrocarbon content. Easy-to-use Windows based software controls the system, is fully programmable and documents the method. With the PowerPrep EPH system you have the option of expanding from one module, that will perform five sample fractionation and cleanups, to a six module system capable of performing 30 sample fractionation and cleanups.
The PowerPrep EPH system delivers the reproducibility you demand by consistently conditioning the columns, delivering the sample to the column fractionates and cleaning up the sample. The PowerPrep EPH system increases sample throughput while reducing errors. It eliminates poor recoveries and provides a cleaner background while eliminating contamination. This system uses FMS’s high quality and inexpensive, Teflon based, pre-packed, disposable columns that deliver high recoveries and eliminate the errors and time spent on manual column packing, gravimetric chromatography and glassware cleanup.
Details
Separates Aliphatic and Aromatic Hydrocarbons
Fractionation is accomplished using either polypropylene cartridges pre-packed with silica gel or glass columns manually packed with conditioned silicagel. While it is difficult to achieve the high aliphatic and aromatic compounds recovery, the manual collection of fractions by using poly-propylene cartridges or manually packed glass columns requires additional time for columnpreparation and calibration. FMS offers a precise method that is automatically controlled by a programmable workstation with patented pre-packed and pre-conditioned columns. Together, they guarantee a consistent level of fractionation and recoveries of targeted compounds.
Fast turnaround: 30 Samples in One Hour
The PowerPrep EPH system increases sample throughput while reducing errors and poor recoveries.
Produces Consistent Reproducible Results
With just a few keystrokes, the PowerPrep EPH system performs an entire column chromatography, automatically achieving high recoveries for all analytes.
Ready-to-Use, Conditioned Columns From FMS
The PowerPrep EPH system uses pre–packed disposable columns made from Teflon and silica. FMS’s columns are tested for purity and performance prior to shipment.
Automates in compliance with Methods MADEP EPH, TNRCC Method 1005-1006
The PowerPrep EPH system is changing high speed sample processing in today’s laboratories. The computer controlled liquid chromatography system performs simultaneous sample processing automatically and unattended. You need only to load your samples, snap on your pre-packed columns and press the start key. The system performs the entire sample cleanup and fractionation according to the MADEP EPH, TNRCC Method 1005-1006 making compliance easy.
Reduce solvent and glassware usage
FMS pre-packed disposable columns eliminate washing glassware and the solvents to clean that glassware.
Dramatically Cuts Operation Costs
Unattended operation of the system saves labor and valuable time. FMS pre-packed columns reduce the need to QC test in the lab as well as errors caused from manual fractionation.
Modular and expandable
With the PowerPrep EPH Fractionation system you have the option to expand from one module, which will perform five sample fractionation and cleanups, to a six module system which will perform 30 sample fractionation and cleanups.
Robust and Easy to Maintain
Both system expansion and module replacement are performed via FMS’s quick connect modules. This feature reduces system down time and increases laboratory throughput.
Cookbook Method
FMS’s powerful windows-based monitoring and control software offers a rich set of features and flexibility, including methods development and optimization. Once the method is optimized it is saved and used for each run, eliminating the need to create a new method each time the system is run. Input parameters include flow rates, volumes, column selection, sample size, solvent selection and fraction collection.
Specifications
Dimensions: 15” W x 18” D x 35” H
Weight: 130 lbs.
Pump: Piston Displacement
Flow rate: 0.2 to 15 mL/minute
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: PC based
SuperVap Concentration System
Dimensions:13” W x 13” D x 12” H
Weight:20 lbs.
Gas Requirements: Nitrogen – 20 PSI minimum
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: Integrated Touch Screen based
Bath: Dry
GPC Clean-up
The PowerPrep GPC System
The PowerPrep GPC™ system is a low cost automated Gel Permeation Chromatography system capable of separating synthetic macromolecules such as pesticides, PCBs, PAHs etc. from interfering compounds. It uses glass or polypropylene columns packed with styrene-divinylbenzene resin beads, and can process from 1 to 30 samples sequentially. The samples are sequentially loaded into the column, then washed and collected in the appropriate fraction vessels. The PowerPrep GPC system greatly simplifies sample cleanup through its unattended operation, increased speed and precision. Options such as different types of columns, a fraction collector, UV detector and a PC allow versatility in a sample type, automatic monitoring, data recording and programmable control over all aspects of the separation procedure
Product Brochure
Details
The PowerPrep EPH High Throughput Sample Fractionation System
Separates Aliphatic and Aromatic Hydrocarbons
Fractionation is accomplished using either polypropylene cartridges pre-packed with silica gel or glass columns manually packed with conditioned silicagel. While it is difficult to achieve the high aliphatic and aromatic compounds recovery, the manual collection of fractions by using poly-propylene cartridges or manually packed glass columns requires additional time for columnpreparation and calibration. FMS offers a precise method that is automatically controlled by a programmable workstation with patented pre-packed and pre-conditioned columns. Together, they guarantee a consistent level of fractionation and recoveries of targeted compounds.
Fast turnaround: 30 Samples in One Hour
The PowerPrep EPH system increases sample throughput while reducing errors and poor recoveries.
Produces Consistent Reproducible Results
With just a few keystrokes, the PowerPrep EPH system performs an entire column chromatography, automatically achieving high recoveries for all analytes.
Ready-to-Use, Conditioned Columns From FMS
The PowerPrep EPH system uses pre–packed disposable columns made from Teflon and silica. FMS’s columns are tested for purity and performance prior to shipment.
Automates in compliance with Methods MADEP EPH, TNRCC Method 1005-1006
The PowerPrep EPH system is changing high speed sample processing in today’s laboratories. The computer controlled liquid chromatography system performs simultaneous sample processing automatically and unattended. You need only to load your samples, snap on your pre-packed columns and press the start key. The system performs the entire sample cleanup and fractionation according to the MADEP EPH, TNRCC Method 1005-1006 making compliance easy.
Reduce solvent and glassware usage
FMS pre-packed disposable columns eliminate washing glassware and the solvents to clean that glassware.
Dramatically Cuts Operation Costs
Unattended operation of the system saves labor and valuable time. FMS pre-packed columns reduce the need to QC test in the lab as well as errors caused from manual fractionation.
Modular and expandable
With the PowerPrep EPH Fractionation system you have the option to expand from one module, which will perform five sample fractionation and cleanups, to a six module system which will perform 30 sample fractionation and cleanups.
Robust and Easy to Maintain
Both system expansion and module replacement are performed via FMS’s quick connect modules. This feature reduces system down time and increases laboratory throughput.
Cookbook Method
FMS’s powerful windows-based monitoring and control software offers a rich set of features and flexibility, including methods development and optimization. Once the method is optimized it is saved and used for each run, eliminating the need to create a new method each time the system is run. Input parameters include flow rates, volumes, column selection, sample size, solvent selection and fraction collection.
Specifications
Dimensions: 15” W x 18” D x 35” H
Weight: 130 lbs.
Pump: Piston Displacement
Flow rate: 0.2 to 15 mL/minute
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: PC based
SuperVap Concentration System
Dimensions:13” W x 13” D x 12” H
Weight:20 lbs.
Gas Requirements: Nitrogen – 20 PSI minimum
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: Integrated Touch Screen based
Bath: Dry
Total Solution Sample Cleanup
Total Rapid Prep System
Total Sample for Prep for Dioxin & PCB – All in one System: Extraction + Clean-up + Concentration
The TRP Total-Rapid-Prep System is the first and only “Total Solution” sample preparation system that combines extraction, sample cleanup, and concentration into one economical package. Designed for efficiency and precision, the TRP system processes up to six samples simultaneously in less than a few hours, delivering the highest recoveries and exceptional results for all target analytes.
Key Features of the TRP Total-Rapid-Prep System
- All-in-One Solution: Combines extraction, cleanup, and concentration in a single system for streamlined workflows.
- Simultaneous Processing: Handles up to six samples at once, reducing turnaround time and boosting productivity.
- Flexible Operation: Offers the option to run individual processes (extraction, cleanup, or concentration) or a combination of all three in a single step.
- Advanced Automation: Controlled by an easy-to-use, Windows-based system that is fully programmable for custom workflows.
- High-Quality Consumables: Utilizes FMS’s prepacked Teflon-based disposable columns, eliminating glassware cleanup and ensuring high recoveries.
- Closed-Loop Design: Prevents cross-contamination and provides a cleaner background for more reliable results.
Modular Design: Three Systems in One Package
The TRP Total-Rapid-Prep System integrates three essential sample preparation modules into a single economical system:
- PLE® – Pressurized Liquid Extraction Module: Efficiently extracts analytes from various sample matrices with high recoveries and reduced solvent usage.
- Power-Prep® – Multi-Column Sample Cleanup Module: Automates multi-column cleanup for enhanced precision and reduced manual labor.
- SuperVap® – Evaporation & Solvent Exchange Module: Concentrates samples and performs solvent exchange directly into autosampler vials, ready for analysis.
Benefits of the TRP Total-Rapid-Prep System
- Increased Throughput: Processes multiple samples simultaneously, allowing laboratories to handle more work in less time.
- Reduced Errors: Automation minimizes human error, ensuring consistent and reproducible results.
- Cost-Effective Operation: Combines three systems into one, saving time and money while delivering excellent performance.
- Improved Efficiency: Runs multiple steps in a single operation, simplifying complex workflows.
- Cleaner Backgrounds: The advanced closed-loop design eliminates contamination, improving the reliability of results.
Applications of the TRP Total-Rapid-Prep System
The TRP system is versatile and ideal for various applications, including:
- Dioxins
- PCBs
- PAHs
- PBDEs
- Pesticides
Why Choose the TRP Total-Rapid-Prep System?
The TRP Total-Rapid-Prep System revolutionizes sample preparation by offering a comprehensive, automated solution that saves time, reduces costs, and improves the accuracy of analytical results. With its ability to perform extraction, cleanup, and concentration in one step, this system is the ultimate choice for laboratories aiming to optimize their workflows and achieve high-quality outcomes.
Product Video
Applications
Analysis of PAHs in PUF filters and Diethylene Glycol-Water Samples with Automated Extraction Cleanup and Concentration
Analysis of PAHs in PUF Filters and Diethylene Glycol-Water Traps by Automated Sample Processing
EPA 1668 PCBs in Coffee via PLE and Reduced Volume Cleanup
EPA 1613 and 1668 Dioxins Furans and PCBs in Peanut Butter Samples by PLE and PowerPrep
EPA 1613 and 1668 Dioxins PCBs and PBDEs in Human Serum by PLE and PowerPrep
EPA 1613 and 1668 PCDDs PCDFs and PCBs in Fish by Automated Sample Processing
EPA 1613 Dioxins and Furans in Crab Meat by PowerPrep and PLE
EPA 1613 Dioxins and Furans in Egg Yolk by PLE
EPA 1613 Dioxins and Furans in Freeze-Dried and Regular Milk by PLE and PowerPrep
EPA 1613 PCDD-Fs and PCBs Analysis in Pet Food Using Automated Extraction and Cleanup
EPA 1613 PCDD-Fs in Cranberry Pulp by PLE and PowerPrep
Cooking up a Solution – Same Day Testing of Dioxins and PCBs for Food Safety is Now Feasible
Details
The Total Rapid Prep™ system
The Total-Rapid-Prep™ system performs complete sample preparation for six GC or GC/MS samples for analysis in a few hours. Solid or semi-solid sample is mixed with drying agent and placed in the extraction cells. The extraction cells are then filled with the solvent(s) of choice. They are pressurized & heated. While the samples are being extracted, the cleanup columns are conditioned. As soon as the extraction cycle is terminated, the extraction columns are depressurized, and flushed with solvent, and then purged with nitrogen. At the moment of the extraction columns depressurization the concentration cycle is started. Solvent exchange (if necessary) is performed for the concentrated sample, and the sample is then transferred to the cleanup columns for purification. As soon as the first fractions start to come off the clean up columns, the concentration cycle starts. The final concentrated fractions are then transferred for GC/MS analysis.
Automated, unattended operation
Just load your samples in the extraction cells, install the extraction cells and cleanup columns on the TRP and press the “RUN” button and the system will perform the entire sample preparation process in virtually one step, automatically and unattended, and deliver the final fractions ready for GC, LC, or GC/LC/MS analysis.
Same day results for multiple samples
Because the Total Rapid Prep system performs extraction, cleanup, and evaporation on one integrated and economical system, it can process up to six samples simultaneously making the same day turnaround of up to 30 samples possible.
Sample preparation for POP analysis made easy
The TRP system uses pre-packed, disposable clean-up columns as well as ready-to-use disposable extraction cell end caps. Because of its integrated design there is no need to transfer samples from one system to another for further processing. This feature allows for “Raw sample in, GC, LC, and GC/LC/MS-ready fraction out”, with minimal need to wash glassware.
Automates EPA SW846 and 40 CFR 136 methods
The Total Rapid Prep system has been approved by the US EPA as an automated alternative to SW-846 and 40 CFR 136 methods for POPs analysis.
Electronic documentation and reporting
The DMS-6000 real-time software plots all the extraction data including six channels of pressure and six channels of temperature plus sample concentration data such as temperature and nitrogen. This allows automatic documentation of the entire sample preparation process. All sample preparation data can be superimposed, reviewed and printed in graphic or tabular format. The DMS-6000 software allows the creation of an automatic data report based on the sample sequence set up. Printed data contains the graph and parameters of the sample preparation.
Reduce solvent and glassware usage
The TRP system utilizes inexpensive pre-packed disposable cleanup columns, filtration cartridges and inexpensive disposable concentration tubes. It can also use disposable extraction cell end caps, greatly reducing the amount of contaminated parts that need to be washed. The efficient manner in which the extraction and cleanup process is performed reduces the volume of solvent used.
Dramatic savings in time and resources
The Total Rapid Prep system increases sample throughput by performing total sample prep in just a few hours per six samples, basically 30-45 minutes per sample, instead of several days. This reduces labor costs.
Low background automated sample prep
TRP Total-Rapid-Prep provides a cleaner background and eliminates cross contamination due to use of pre-packed disposable columns as well as its advanced closed loop system design.
Wide range of inexpensive extraction cell sizes
A wide range of inexpensive stainless steel extraction cell sizes are available for the Total-Prep™. Currently available sizes include 5 mL, 10 mL, 20 mL, 40 mL, 70 mL, and 100 mL. They are made of either stainless steel 316, or the special acid and alkali resistant alloy stainless steel. With its flexible design and construction the Total Rapid Prep system can accommodate the whole range of extraction cell sizes; from the 5 mL cell all the way to the 100 mL, in the same system.
Wide range of pre-packed disposable clean up columns
A wide variety of pre-packed disposable clean up columns are available. These cleanup columns vary in size and packing material types from standard multi-layered A-B-N silica to the special and custom made.
Disposable Columns used for Dioxins and PCBs, PBDEs analysis:
- Multi-layered A-B-N silica
- Alumina
- Carbon
- High capacity acid silica (optional used for fatty samples, this column removes 3-5 grams fat
Disposable or reusable extraction filtration end caps
The Total Rapid Prep system’s extraction cells can be used with either disposable Teflon end caps or stainless steel reusable end caps. In high throughput laboratories where fast sample turn-around time is the goal, the disposable Teflon end caps may be used to save end cap washing and assembly time. The reusable stainless steel end caps may be used when saving time and labor is not the overriding issue.
Modular and expandable
The Total Rapid Prep system’s modular design is expandable from one to six sample configurations. The modular and flexible design of the TRP system allows laboratories to acquire a one sample configuration system inexpensively and expand it to 2, 3, 4, 5, or a 6 sample configuration as demand for higher sample throughput grows. The system’s modular design makes expansions extremely easy and fast. Laboratory personnel can easily add the expansion modules on sight by connecting them to the existing system in less than an hour. The modular design of the TRP system makes it easy to expand and maintain.
A tool for method development
The Total Rapid Prep system is the best method development tool for today’s laboratories. It is capable of utilizing a wide range of extraction cell sizes, cleanup columns, and multiple solvent selection valves. Along with the flexible DMS6000 software the TRP system is an extremely capable tool for experimenting with different sample sizes, solvents, flow rates, cleanup packing materials, extraction pressures and temperatures.
Specifications
Pressurized Liquid Extraction System
Dimensions: 15” W X 18” D X 35” H
Weight: 140 lbs
Flow Rate: 0 – 35 mL/minute
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: PC based
PowerPrep MultiColumn Cleanup System
Dimensions: 15” W x 18” D x 35” H
Weight: 130 lbs.
Pump: Piston Displacement
Flow rate: 0.2 to 15 mL/minute
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: PC based
SuperVap Concentrator
Dimensions: 13” W x 13” D x 12” H
Weight: 20 lbs.
Gas Requirements: Nitrogen – 20 PSI minimum
Electrical Input: 110/220 Volts, 50/60 HZ
Controller: PC based
Bath: Dry
Consumables
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Simple, Quick, Powerful - Automated Dioxins/PCBs Sample CleanUp
Automated EZprep+ Sample Cleanup System
Features and Benefits:
| Simple to Run | 3 Easy Steps to run the entire CleanUp Process |
| Fast | 30 to 45 minutes |
| Green Technology | Zero DCM |
| Closed System | No Exposure to harmful Chemicals |
| High Throughput | 1 to 6 Samples in Parallel |
| Low Solvent | As Low As 110ml per Sample |
| Reliable | No Downtime, No Computer or Electromechanical valves to fail |
| High Fat Capacity | Up to 5 Grams (7 grams for special orders) |
| Quality Consumables | Guaranteed Certified Columns |
| Economical | Column Kits to meet your Sample Matrix |
Product Video
Application Notes
Applications
| Solids: | Liquids: |
| Fish | Milk |
| Feed | Oil |
| Meat | Serum |
| Soil | Water |
| Fly Ash | Waste Water |
Specifications
Coming Soon.
Consumables
| Part Number | Includes | Description |
| EHCLS-KT05.0DP | Extra High Capacity DIOXIN/PCB Kit 5g Fat Removal Capacity | |
| SNEH-ACD-050 | Extra High Capacity Acid Silica Column | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNAL-BAS-006 | 6G Basic Alumina Column | |
| SNCA-C45-034 | Carbon/Celite Column | |
| HCCLS-KT2.5DP | High Capacity DIOXIN/PCB Kit 2.5 Fat Removal Capacity | |
| SNHC-ACD-029 | High Capacity Acid Silica Columns | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNAL-BAS-006 | 6G Basic Alumina Column | |
| SNCA-C45-034 | Carbon/Celite Column | |
| MIDLS-KT1.0DP | Classical Plus DIOXIN/PCB Kit 1g Fat Removal Capacity | |
| SNMI-ACD-009 | Medium Capacity Acid Silica Column | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNCL-BAS-004 | 4G Basic Alumina Column | |
| SNCA-C70-034 | Carbon/Celite Column | |
| CLSLS-KT0.5DP | Classical DIOXIN/PCB Kit .5g Fat Removal Capacity | |
| SNCL-ACD-006 | Classical Acid Silica Column | |
| SNLC-BAN-004 | Basic and Neutral Silica Column | |
| SNCL-BAS-004 | 4G Basic Alumina Column | |
| SNCA-C70-034 | Carbon/Celite Column |